data_global _audit_creation_method 'APEX3 v2017.3-0' _publ_requested_journal ? _publ_contact_author_name ? _publ_contact_author_address ; ; _publ_contact_author_email ? _publ_contact_author_fax ? _publ_contact_author_phone ? _publ_section_title ; ; _publ_section_abstract ; ; _publ_section_references ; ; _publ_section_comment ; ; data_20190822tengchongU2 _chemical_name_systematic ? _chemical_name_common CaMoUOH _chemical_formula_moiety ? _chemical_formula_sum 'Ca0.96 Mo2 O37 U6' _chemical_formula_iupac ? _chemical_formula_weight 2250.54 _chemical_absolute_configuration ? _chemical_melting_point ? _space_group_crystal_system orthorhombic _space_group_name_H-M_alt 'C 2 2 21' _space_group_name_Hall 'C 2c 2' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' '-x, y, -z+1/2' 'x, -y, -z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z+1/2' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' _cell_length_a 13.0866(8) _cell_length_b 17.6794(12) _cell_length_c 15.6800(9) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 3627.8(4) _cell_formula_units_Z 4 _cell_measurement_reflns_used 1976 _cell_measurement_theta_min 2.3054 _cell_measurement_theta_max 31.7733 _cell_measurement_temperature 293.(2) _exptl_crystal_description plank _exptl_crystal_colour 'translucent light yellow' _exptl_crystal_size_max 0.050 _exptl_crystal_size_mid 0.050 _exptl_crystal_size_min 0.030 _exptl_crystal_density_diffrn 4.121 _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 3805 _exptl_absorpt_coefficient_mu 27.592 _exptl_absorpt_correction_type Multi-Scan _exptl_absorpt_process_details ; SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction ; _exptl_absorpt_correction_T_min 0.23 _exptl_absorpt_correction_T_max 0.49 _exptl_special_details ; ; _diffrn_ambient_temperature 293.(2) _diffrn_source 'Incoatec Ims 2.0' _diffrn_source_type Microfocus _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator 'multi layer optic' _diffrn_measurement_device_type 'Bruker D8 QUEST PHOTON 100' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean 10.4167 _diffrn_reflns_number 49381 _diffrn_reflns_av_R_equivalents 0.0592 _diffrn_reflns_av_unetI/netI 0.0466 _diffrn_reflns_theta_min 2.33 _diffrn_reflns_theta_max 33.26 _diffrn_reflns_theta_full 33.26 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measured_fraction_theta_full 0.998 _diffrn_reflns_limit_h_min -20 _diffrn_reflns_limit_h_max 20 _diffrn_reflns_limit_k_min -27 _diffrn_reflns_limit_k_max 27 _diffrn_reflns_limit_l_min -24 _diffrn_reflns_limit_l_max 24 _refine_special_details ; ; _reflns_number_total 6965 _reflns_number_gt 6055 _reflns_threshold_expression 'I > 2\s(I)' _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_R_factor_all 0.0442 _refine_ls_R_factor_gt 0.0323 _refine_ls_wR_factor_gt 0.0642 _refine_ls_wR_factor_ref 0.0671 _refine_ls_goodness_of_fit_ref 1.051 _refine_ls_restrained_S_all 1.051 _refine_ls_number_reflns 6965 _refine_ls_number_parameters 198 _refine_ls_number_restraints 0 _refine_ls_number_constraints ? _refine_ls_hydrogen_treatment undef _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0321P)^2^+0.9966P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_hydrogens ? _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_diff_density_max 2.609 _refine_diff_density_min -1.138 _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_abs_structure_details ; Flack x determined using 2424 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.016(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Ca Ca 0.2262 0.3064 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' U U -9.6767 9.6646 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _computing_data_collection ? _computing_cell_refinement 'APEX3 v2017.3-0 (Bruker AXS)' _computing_data_reduction 'SAINT V8.38A (Bruker AXS Inc., 2017)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2016/6 (Sheldrick, 2016)' _computing_molecular_graphics 'shelXle (C.B. Huebschle, rev 833)' _computing_publication_material ? loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_refinement_flags_posn _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group U U1 0.74960(3) 0.27093(2) 0.48457(2) 0.01991(9) Uani d . . . 1 . . U U2 0.77624(3) 0.20695(2) 0.25350(2) 0.01830(8) Uani d . . . 1 . . U U3 0.52535(3) 0.17391(2) 0.37445(2) 0.01862(8) Uani d . . . 1 . . Mo Mo 1.00222(6) 0.30274(6) 0.39165(5) 0.02016(17) Uani d . . . 1 . . Ca Ca 0.8926(4) 0.1102(3) 0.6439(4) 0.0349(12) Uani d . P . 0.48 . . O O1 0.6986(6) 0.3545(5) 0.4355(5) 0.0301(19) Uani d . . . 1 . . O O2 0.8036(6) 0.1906(6) 0.5379(5) 0.033(2) Uani d . . . 1 . . O O3 0.7162(6) 0.2953(5) 0.2290(5) 0.0311(19) Uani d . . . 1 . . O O4 0.8339(6) 0.1185(5) 0.2742(5) 0.0322(19) Uani d . . . 1 . . O O5 0.4964(7) 0.2701(5) 0.3518(5) 0.0295(16) Uani d . . . 1 . . O O6 0.5500(6) 0.0768(6) 0.3940(5) 0.0328(19) Uani d . . . 1 . . O O7 0.9247(6) 0.2629(6) 0.1891(5) 0.038(2) Uani d . . . 1 . . O O8 0.8762(5) 0.2622(5) 0.3711(5) 0.0247(16) Uani d . . . 1 . . O O9 1.0048(8) 0.3981(5) 0.3705(6) 0.042(2) Uani d . . . 1 . . O O10 1.0794(5) 0.2776(5) 0.4845(5) 0.0262(17) Uani d . . . 1 . . O O11 0.6897(5) 0.2015(5) 0.3759(4) 0.0238(15) Uani d . . . 1 . . O O12 0.4038(5) 0.1601(5) 0.4868(5) 0.0254(17) Uani d . . . 1 . . O O13 0.6064(5) 0.1467(4) 0.2311(4) 0.0176(15) Uani d . . . 1 . . O O14 0.7201(5) 0.3298(5) 0.6124(4) 0.0251(15) Uani d . . . 1 . . O O15W 0.9873(15) 0.0996(11) 0.5169(13) 0.045(4) Uiso d . P . 0.5 . . O O16W 0.731(2) 0.0505(15) 0.6180(17) 0.077(7) Uiso d . P . 0.5 . . O O17W 0.945(2) -0.0217(16) 0.6328(18) 0.073(8) Uiso d . P . 0.5 . . O O18W 0.914(2) 0.0884(19) 0.793(2) 0.089(9) Uiso d . P . 0.5 . . O O19W 0.3830(14) 0 0.5 0.073(5) Uiso d . P S 1 . . O O20W 0.6418(11) -0.0049(10) 0.2128(10) 0.087(4) Uiso d . . . 1 . . O O21W 0.6741(15) 0.4763(12) 0.5960(13) 0.126(7) Uiso d . . . 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 U1 0.01388(14) 0.0353(2) 0.01053(13) -0.00152(14) -0.00023(12) -0.00047(14) U2 0.01477(14) 0.02956(19) 0.01057(13) 0.00037(13) 0.00067(12) -0.00013(16) U3 0.01421(15) 0.0288(2) 0.01288(14) -0.00069(14) 0.00018(12) 0.00061(16) Mo 0.0123(3) 0.0361(5) 0.0121(3) 0.0009(3) -0.0014(3) 0.0010(3) Ca 0.034(3) 0.030(3) 0.041(3) 0.003(2) 0.006(2) -0.001(2) O1 0.034(4) 0.039(5) 0.017(3) 0.008(4) 0.003(3) 0.008(3) O2 0.034(4) 0.047(6) 0.017(4) 0.003(4) -0.004(3) -0.001(4) O3 0.031(4) 0.029(4) 0.033(4) 0.002(4) -0.004(3) 0.008(3) O4 0.035(4) 0.037(5) 0.025(4) 0.009(4) -0.001(3) 0.002(4) O5 0.034(4) 0.028(4) 0.027(4) 0.006(4) -0.006(3) 0.005(3) O6 0.033(4) 0.038(5) 0.028(4) 0.001(4) 0.006(3) 0.007(4) O7 0.023(4) 0.072(7) 0.018(4) -0.019(4) -0.003(3) 0.008(4) O8 0.012(3) 0.046(5) 0.016(3) -0.008(3) 0.001(2) 0.000(4) O9 0.048(5) 0.043(5) 0.035(5) -0.009(5) 0.004(5) 0.007(4) O10 0.017(3) 0.050(5) 0.012(3) 0.006(3) -0.002(2) -0.004(3) O11 0.020(3) 0.042(5) 0.010(3) -0.008(3) 0.004(2) -0.005(3) O12 0.018(3) 0.043(5) 0.015(3) 0.000(3) 0.005(3) 0.003(3) O13 0.012(3) 0.027(4) 0.013(3) 0.003(3) 0.000(2) 0.001(3) O14 0.023(3) 0.037(4) 0.015(3) -0.002(3) -0.001(3) 0.000(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag U1 O2 . 1.792(9) ? U1 O1 . 1.795(8) ? U1 O11 . 2.241(7) ? U1 O14 . 2.291(7) ? U1 O12 8_556 2.401(7) ? U1 O8 . 2.436(7) ? U1 O10 8_456 2.436(7) ? U1 Mo . 3.6563(9) ? U1 U2 . 3.8117(6) ? U1 U3 . 3.8125(5) ? U1 Ca . 4.221(6) ? U2 O4 . 1.766(9) ? U2 O3 . 1.790(8) ? U2 O11 . 2.231(7) ? U2 O14 6_654 2.307(7) ? U2 O7 . 2.403(8) ? U2 O8 . 2.464(7) ? U2 O13 . 2.490(7) ? U2 U3 . 3.8364(5) ? U3 O6 . 1.773(10) ? U3 O5 . 1.779(8) ? U3 O11 . 2.205(7) ? U3 O12 . 2.386(7) ? U3 O13 3_655 2.438(6) ? U3 O10 8_456 2.474(7) ? U3 O13 . 2.531(6) ? U3 U3 3_655 3.9588(7) ? U3 Ca 8_456 4.203(6) ? Mo O9 . 1.718(9) ? Mo O7 3_755 1.737(8) ? Mo O8 . 1.826(7) ? Mo O10 . 1.827(7) ? Mo O12 8_556 2.392(8) ? Ca O15W . 2.35(2) ? Ca O18W . 2.39(3) ? Ca O16W . 2.39(3) ? Ca O17W . 2.44(3) ? Ca O2 . 2.479(10) ? Ca O5 8_556 2.515(10) ? Ca O3 6_655 2.569(10) ? Ca O18W 3_756 2.74(3) ? Ca Ca 3_756 4.355(12) ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O2 U1 O1 . . 176.9(4) ? O2 U1 O11 . . 93.4(3) ? O1 U1 O11 . . 89.7(4) ? O2 U1 O14 . . 91.1(3) ? O1 U1 O14 . . 86.4(3) ? O11 U1 O14 . . 148.8(2) ? O2 U1 O12 . 8_556 89.1(3) ? O1 U1 O12 . 8_556 88.5(3) ? O11 U1 O12 . 8_556 135.6(3) ? O14 U1 O12 . 8_556 75.3(3) ? O2 U1 O8 . . 91.3(3) ? O1 U1 O8 . . 89.5(3) ? O11 U1 O8 . . 69.4(2) ? O14 U1 O8 . . 141.4(3) ? O12 U1 O8 8_556 . 66.2(3) ? O2 U1 O10 . 8_456 89.3(3) ? O1 U1 O10 . 8_456 92.0(3) ? O11 U1 O10 . 8_456 68.8(2) ? O14 U1 O10 . 8_456 80.4(3) ? O12 U1 O10 8_556 8_456 155.6(3) ? O8 U1 O10 . 8_456 138.2(3) ? O2 U1 Mo . . 87.2(3) ? O1 U1 Mo . . 92.2(3) ? O11 U1 Mo . . 95.60(17) ? O14 U1 Mo . . 115.51(18) ? O12 U1 Mo 8_556 . 40.19(19) ? O8 U1 Mo . . 26.32(17) ? O10 U1 Mo 8_456 . 163.80(19) ? O2 U1 U2 . . 99.9(3) ? O1 U1 U2 . . 82.6(3) ? O11 U1 U2 . . 31.45(17) ? O14 U1 U2 . . 169.0(2) ? O12 U1 U2 8_556 . 104.57(18) ? O8 U1 U2 . . 39.19(16) ? O10 U1 U2 8_456 . 99.68(17) ? Mo U1 U2 . . 65.429(15) ? O2 U1 U3 . . 99.1(3) ? O1 U1 U3 . . 83.7(3) ? O11 U1 U3 . . 30.70(17) ? O14 U1 U3 . . 118.11(18) ? O12 U1 U3 8_556 . 163.83(18) ? O8 U1 U3 . . 99.47(17) ? O10 U1 U3 8_456 . 39.43(17) ? Mo U1 U3 . . 125.783(17) ? U2 U1 U3 . . 60.422(9) ? O2 U1 Ca . . 10.3(3) ? O1 U1 Ca . . 166.6(3) ? O11 U1 Ca . . 103.7(2) ? O14 U1 Ca . . 82.1(2) ? O12 U1 Ca 8_556 . 81.9(2) ? O8 U1 Ca . . 95.0(2) ? O10 U1 Ca 8_456 . 92.9(2) ? Mo U1 Ca . . 86.48(8) ? U2 U1 Ca . . 108.81(8) ? U3 U1 Ca . . 107.85(8) ? O4 U2 O3 . . 178.0(4) ? O4 U2 O11 . . 91.2(3) ? O3 U2 O11 . . 90.0(3) ? O4 U2 O14 . 6_654 85.3(3) ? O3 U2 O14 . 6_654 92.8(3) ? O11 U2 O14 . 6_654 145.5(3) ? O4 U2 O7 . . 95.5(4) ? O3 U2 O7 . . 84.6(4) ? O11 U2 O7 . . 142.2(3) ? O14 U2 O7 6_654 . 72.3(3) ? O4 U2 O8 . . 89.2(4) ? O3 U2 O8 . . 92.8(3) ? O11 U2 O8 . . 69.1(2) ? O14 U2 O8 6_654 . 145.0(2) ? O7 U2 O8 . . 73.8(2) ? O4 U2 O13 . . 91.7(3) ? O3 U2 O13 . . 87.2(3) ? O11 U2 O13 . . 69.5(2) ? O14 U2 O13 6_654 . 76.3(2) ? O7 U2 O13 . . 147.0(2) ? O8 U2 O13 . . 138.5(2) ? O4 U2 U1 . . 97.3(3) ? O3 U2 U1 . . 84.6(3) ? O11 U2 U1 . . 31.62(19) ? O14 U2 U1 6_654 . 175.82(18) ? O7 U2 U1 . . 110.6(2) ? O8 U2 U1 . . 38.67(15) ? O13 U2 U1 . . 100.32(15) ? O4 U2 U3 . . 98.1(3) ? O3 U2 U3 . . 82.1(3) ? O11 U2 U3 . . 29.95(18) ? O14 U2 U3 6_654 . 116.67(18) ? O7 U2 U3 . . 164.3(3) ? O8 U2 U3 . . 98.33(15) ? O13 U2 U3 . . 40.57(15) ? U1 U2 U3 . . 59.800(10) ? O6 U3 O5 . . 177.6(4) ? O6 U3 O11 . . 92.0(3) ? O5 U3 O11 . . 89.9(4) ? O6 U3 O12 . . 83.9(3) ? O5 U3 O12 . . 95.9(3) ? O11 U3 O12 . . 131.7(3) ? O6 U3 O13 . 3_655 93.2(3) ? O5 U3 O13 . 3_655 84.4(3) ? O11 U3 O13 . 3_655 137.7(2) ? O12 U3 O13 . 3_655 90.6(2) ? O6 U3 O10 . 8_456 97.4(3) ? O5 U3 O10 . 8_456 84.7(3) ? O11 U3 O10 . 8_456 68.6(2) ? O12 U3 O10 . 8_456 64.3(2) ? O13 U3 O10 3_655 8_456 151.3(2) ? O6 U3 O13 . . 83.9(3) ? O5 U3 O13 . . 95.4(3) ? O11 U3 O13 . . 69.1(2) ? O12 U3 O13 . . 156.3(3) ? O13 U3 O13 3_655 . 69.9(2) ? O10 U3 O13 8_456 . 137.7(2) ? O6 U3 U1 . . 102.5(3) ? O5 U3 U1 . . 79.9(3) ? O11 U3 U1 . . 31.25(19) ? O12 U3 U1 . . 102.99(19) ? O13 U3 U1 3_655 . 160.14(17) ? O10 U3 U1 8_456 . 38.71(15) ? O13 U3 U1 . . 99.51(15) ? O6 U3 U2 . . 94.4(3) ? O5 U3 U2 . . 86.4(3) ? O11 U3 U2 . . 30.33(18) ? O12 U3 U2 . . 162.01(18) ? O13 U3 U2 3_655 . 107.42(15) ? O10 U3 U2 8_456 . 98.31(15) ? O13 U3 U2 . . 39.78(15) ? U1 U3 U2 . . 59.778(10) ? O6 U3 U3 . 3_655 101.6(3) ? O5 U3 U3 . 3_655 76.5(2) ? O11 U3 U3 . 3_655 100.00(18) ? O12 U3 U3 . 3_655 128.04(18) ? O13 U3 U3 3_655 3_655 38.00(15) ? O10 U3 U3 8_456 3_655 158.25(19) ? O13 U3 U3 . 3_655 36.38(14) ? U1 U3 U3 . 3_655 125.134(13) ? U2 U3 U3 . 3_655 69.884(11) ? O6 U3 Ca . 8_456 165.0(3) ? O5 U3 Ca . 8_456 14.0(3) ? O11 U3 Ca . 8_456 101.7(2) ? O12 U3 Ca . 8_456 82.4(2) ? O13 U3 Ca 3_655 8_456 80.81(19) ? O10 U3 Ca 8_456 8_456 82.2(2) ? O13 U3 Ca . 8_456 106.55(18) ? U1 U3 Ca . 8_456 86.60(8) ? U2 U3 Ca . 8_456 100.46(8) ? U3 U3 Ca 3_655 8_456 82.13(8) ? O9 Mo O7 . 3_755 104.3(5) ? O9 Mo O8 . . 111.6(5) ? O7 Mo O8 3_755 . 102.1(4) ? O9 Mo O10 . . 112.4(4) ? O7 Mo O10 3_755 . 100.3(3) ? O8 Mo O10 . . 122.9(3) ? O9 Mo O12 . 8_556 83.9(4) ? O7 Mo O12 3_755 8_556 171.5(4) ? O8 Mo O12 . 8_556 76.2(3) ? O10 Mo O12 . 8_556 74.3(3) ? O9 Mo U1 . . 104.2(4) ? O7 Mo U1 3_755 . 136.6(3) ? O8 Mo U1 . . 36.3(2) ? O10 Mo U1 . . 98.3(2) ? O12 Mo U1 8_556 . 40.37(18) ? O15W Ca O18W . . 138.9(9) ? O15W Ca O16W . . 106.6(8) ? O18W Ca O16W . . 101.5(10) ? O15W Ca O17W . . 73.4(8) ? O18W Ca O17W . . 83.2(10) ? O16W Ca O17W . . 79.4(9) ? O15W Ca O2 . . 74.1(5) ? O18W Ca O2 . . 143.7(8) ? O16W Ca O2 . . 74.0(7) ? O17W Ca O2 . . 129.4(7) ? O15W Ca O5 . 8_556 78.8(5) ? O18W Ca O5 . 8_556 92.6(8) ? O16W Ca O5 . 8_556 148.4(7) ? O17W Ca O5 . 8_556 130.8(7) ? O2 Ca O5 . 8_556 77.8(3) ? O15W Ca O3 . 6_655 141.5(6) ? O18W Ca O3 . 6_655 70.2(8) ? O16W Ca O3 . 6_655 83.5(7) ? O17W Ca O3 . 6_655 144.7(7) ? O2 Ca O3 . 6_655 73.4(3) ? O5 Ca O3 8_556 6_655 74.8(3) ? O15W Ca O18W . 3_756 78.9(8) ? O18W Ca O18W . 3_756 61.0(12) ? O16W Ca O18W . 3_756 144.3(10) ? O17W Ca O18W . 3_756 68.2(10) ? O2 Ca O18W . 3_756 139.1(7) ? O5 Ca O18W 8_556 3_756 67.1(7) ? O3 Ca O18W 6_655 3_756 114.6(7) ? O15W Ca U3 . 8_556 78.3(5) ? O18W Ca U3 . 8_556 99.5(8) ? O16W Ca U3 . 8_556 138.8(7) ? O17W Ca U3 . 8_556 138.3(6) ? O2 Ca U3 . 8_556 68.1(3) ? O5 Ca U3 8_556 8_556 9.9(2) ? O3 Ca U3 6_655 8_556 71.0(2) ? O18W Ca U3 3_756 8_556 76.8(7) ? O15W Ca U1 . . 77.6(5) ? O18W Ca U1 . . 137.8(8) ? O16W Ca U1 . . 78.8(7) ? O17W Ca U1 . . 136.7(7) ? O2 Ca U1 . . 7.4(2) ? O5 Ca U1 8_556 . 71.9(2) ? O3 Ca U1 6_655 . 67.9(2) ? O18W Ca U1 3_756 . 135.8(7) ? U3 Ca U1 8_556 . 62.06(8) ? O15W Ca Ca . 3_756 107.9(5) ? O18W Ca Ca . 3_756 34.4(8) ? O16W Ca Ca . 3_756 134.3(7) ? O17W Ca Ca . 3_756 82.6(7) ? O2 Ca Ca . 3_756 144.7(3) ? O5 Ca Ca 8_556 3_756 68.3(2) ? O3 Ca Ca 6_655 3_756 87.8(3) ? O18W Ca Ca 3_756 3_756 29.5(7) ? U3 Ca Ca 8_556 3_756 77.62(9) ? U1 Ca Ca . 3_756 137.58(8) ? U1 O2 Ca . . 162.2(5) ? U2 O3 Ca . 6_654 157.3(5) ? U3 O5 Ca . 8_456 156.1(5) ? Mo O7 U2 3_755 . 156.7(4) ? Mo O8 U1 . . 117.4(3) ? Mo O8 U2 . . 140.1(4) ? U1 O8 U2 . . 102.1(2) ? Mo O10 U1 . 8_556 138.6(4) ? Mo O10 U3 . 8_556 118.1(3) ? U1 O10 U3 8_556 8_556 101.9(3) ? U3 O11 U2 . . 119.7(3) ? U3 O11 U1 . . 118.0(3) ? U2 O11 U1 . . 116.9(3) ? U3 O12 Mo . 8_456 101.6(3) ? U3 O12 U1 . 8_456 130.3(4) ? Mo O12 U1 8_456 8_456 99.4(3) ? U3 O13 U2 3_655 . 130.0(3) ? U3 O13 U3 3_655 . 105.6(2) ? U2 O13 U3 . . 99.7(2) ? U1 O14 U2 . 6_655 135.0(4) ? Ca O18W Ca . 3_756 116.0(12) ? _shelx_res_file ; TITL Teng in C222(1) teng.res created by SHELXL-2016/6 at 09:25:47 on 18-Jun-2020 CELL 0.71073 13.0866 17.6794 15.6800 90.000 90.000 90.000 ZERR 4.000 0.0008 0.0012 0.0009 0.000 0.000 0.000 LATT -7 SYMM -X, -Y, 1/2+Z SYMM -X, Y, 1/2-Z SYMM X, -Y, -Z SFAC CA MO O U UNIT 3.84 8 148 24 L.S. 10 BOND LIST 4 ACTA FMAP 2 PLAN 20 SIZE 0.05 0.05 0.03 OMIT 1 3 1 OMIT -1 3 1 OMIT 0 0 4 WGHT 0.032100 0.996600 FVAR 0.05081 U1 4 0.749598 0.270933 0.484569 11.00000 0.01388 0.03531 = 0.01053 -0.00047 -0.00023 -0.00152 U2 4 0.776240 0.206950 0.253498 11.00000 0.01477 0.02956 = 0.01057 -0.00013 0.00067 0.00037 U3 4 0.525354 0.173910 0.374453 11.00000 0.01421 0.02878 = 0.01288 0.00061 0.00018 -0.00069 MO 2 1.002220 0.302743 0.391655 11.00000 0.01225 0.03613 = 0.01211 0.00100 -0.00143 0.00089 CA 1 0.892589 0.110222 0.643919 10.48000 0.03362 0.03029 = 0.04070 -0.00075 0.00580 0.00255 O1 3 0.698614 0.354526 0.435502 11.00000 0.03406 0.03923 = 0.01702 0.00847 0.00270 0.00813 O2 3 0.803552 0.190647 0.537875 11.00000 0.03425 0.04664 = 0.01726 -0.00081 -0.00400 0.00276 O3 3 0.716184 0.295252 0.228985 11.00000 0.03138 0.02937 = 0.03267 0.00813 -0.00380 0.00192 O4 3 0.833934 0.118504 0.274189 11.00000 0.03472 0.03706 = 0.02468 0.00235 -0.00073 0.00865 O5 3 0.496405 0.270144 0.351784 11.00000 0.03355 0.02811 = 0.02671 0.00470 -0.00631 0.00552 O6 3 0.550005 0.076813 0.394005 11.00000 0.03257 0.03822 = 0.02771 0.00737 0.00617 0.00147 O7 3 0.924728 0.262884 0.189141 11.00000 0.02292 0.07203 = 0.01769 0.00843 -0.00263 -0.01861 O8 3 0.876241 0.262203 0.371135 11.00000 0.01201 0.04597 = 0.01601 -0.00044 0.00102 -0.00839 O9 3 1.004808 0.398101 0.370524 11.00000 0.04824 0.04294 = 0.03505 0.00703 0.00415 -0.00897 O10 3 1.079359 0.277617 0.484538 11.00000 0.01668 0.05013 = 0.01167 -0.00354 -0.00169 0.00558 O11 3 0.689685 0.201525 0.375909 11.00000 0.01956 0.04192 = 0.00979 -0.00451 0.00374 -0.00759 O12 3 0.403827 0.160073 0.486807 11.00000 0.01833 0.04258 = 0.01533 0.00296 0.00529 0.00033 O13 3 0.606377 0.146705 0.231136 11.00000 0.01203 0.02729 = 0.01348 0.00131 -0.00041 0.00251 O14 3 0.720144 0.329840 0.612357 11.00000 0.02339 0.03743 = 0.01458 0.00048 -0.00070 -0.00199 O15W 3 0.987300 0.099646 0.516856 10.50000 0.04500 O16W 3 0.731352 0.050531 0.617993 10.50000 0.07721 O17W 3 0.945478 -0.021740 0.632838 10.50000 0.07345 O18W 3 0.914195 0.088401 0.793192 10.50000 0.08913 O19W 3 0.383011 0.000000 0.500000 10.50000 0.07301 O20W 3 0.641808 -0.004934 0.212781 11.00000 0.08670 O21W 3 0.674063 0.476317 0.595980 11.00000 0.12563 HKLF 4 REM Teng in C222(1) REM R1 = 0.0323 for 6055 Fo > 4sig(Fo) and 0.0442 for all 6965 data REM 198 parameters refined using 0 restraints END WGHT 0.0321 0.9813 REM Highest difference peak 2.609, deepest hole -1.138, 1-sigma level 0.286 Q1 1 0.5252 0.2213 0.3747 11.00000 0.05 2.61 Q2 1 0.7785 0.2544 0.2523 11.00000 0.05 2.50 Q3 1 0.7553 0.2268 0.4857 11.00000 0.05 2.38 Q4 1 0.7772 0.1589 0.2534 11.00000 0.05 2.38 Q5 1 0.5248 0.1265 0.3710 11.00000 0.05 2.26 Q6 1 0.7527 0.3180 0.4854 11.00000 0.05 2.22 Q7 1 0.8367 0.0537 0.7782 11.00000 0.05 1.84 Q8 1 0.7169 0.0564 0.6513 11.00000 0.05 1.40 Q9 1 0.9948 -0.0547 0.6420 11.00000 0.05 1.36 Q10 1 1.0052 0.2604 0.3953 11.00000 0.05 1.30 Q11 1 0.6199 -0.0073 0.2393 11.00000 0.05 1.27 Q12 1 0.9525 0.0986 0.7724 11.00000 0.05 1.23 Q13 1 1.0176 0.3599 0.3750 11.00000 0.05 1.20 Q14 1 0.9945 0.0826 0.5417 11.00000 0.05 1.20 Q15 1 0.7373 0.0466 0.5872 11.00000 0.05 1.19 Q16 1 0.9686 0.1083 0.4903 11.00000 0.05 1.16 Q17 1 0.5788 0.1685 0.3837 11.00000 0.05 1.10 Q18 1 0.6831 -0.0531 0.2256 11.00000 0.05 1.09 Q19 1 0.8040 0.2690 0.4742 11.00000 0.05 0.99 Q20 1 0.6591 0.0100 0.1819 11.00000 0.05 0.98 ; _shelx_res_checksum 95773 _shelx_hkl_file ; 2 0 0 265.67 14.40 2 0 0 272.37 14.60 -2 0 0 269.67 14.30 -2 0 0 267.27 14.30 -2 0 0 255.17 14.40 -2 0 0 269.37 14.60 2 0 0 269.27 14.30 2 0 0 271.97 14.30 4 0 0 6803.32 360.06 -4 0 0 7131.69 360.16 -6 0 0 201.28 11.90 -6 0 0 207.98 13.10 -6 0 0 199.48 12.30 6 0 0 202.88 11.90 6 0 0 194.68 12.50 6 0 0 206.08 12.40 6 0 0 194.88 12.80 6 0 0 191.18 11.90 8 0 0 1845.62 97.49 8 0 0 1887.41 97.39 8 0 0 1807.22 97.89 -8 0 0 1821.92 96.59 -8 0 0 1834.52 98.09 8 0 0 1795.92 96.79 -8 0 0 1897.61 96.79 8 0 0 1841.02 96.69 10 0 0 22.30 5.00 10 0 0 19.40 3.90 10 0 0 25.20 4.60 10 0 0 7.00 3.80 10 0 0 15.30 4.20 -10 0 0 14.00 6.30 -10 0 0 11.20 4.00 -10 0 0 17.50 4.20 -12 0 0 127.79 10.90 -12 0 0 133.39 10.40 12 0 0 112.99 11.30 12 0 0 128.29 10.70 12 0 0 126.39 12.30 -14 0 0 33.10 6.40 14 0 0 35.00 8.10 -14 0 0 41.60 8.60 14 0 0 47.60 8.20 -16 0 0 9.60 6.30 16 0 0 4.30 6.70 16 0 0 3.10 6.70 18 0 0 8.50 8.80 -18 0 0 28.50 8.40 18 0 0 24.90 9.10 -20 0 0 7.00 10.50 20 0 0 8.20 12.80 20 0 0 9.60 10.70 -3 -1 0 649.54 33.60 -3 -1 0 650.43 34.00 3 -1 0 642.24 33.90 3 -1 0 636.14 33.80 -3 -1 0 596.34 33.40 3 -1 0 660.23 33.40 -3 -1 0 616.24 33.60 3 -1 0 623.44 33.50 3 -1 0 639.14 33.70 -3 1 0 626.44 33.40 3 1 0 631.64 33.60 3 1 0 618.04 33.90 3 1 0 643.54 33.50 -3 1 0 657.63 33.90 -3 1 0 645.14 33.40 3 1 0 623.64 33.60 -5 -1 0 1.30 2.00 -5 -1 0 1.80 1.70 5 -1 0 2.00 1.50 -5 -1 0 3.70 1.80 -5 -1 0 4.20 2.30 5 -1 0 1.20 1.90 5 -1 0 3.30 2.10 5 -1 0 4.90 2.60 -5 1 0 4.60 2.40 5 1 0 3.30 1.70 -5 1 0 3.60 1.70 5 1 0 2.50 1.70 5 1 0 1.60 2.30 -5 1 0 2.70 1.60 -7 -1 0 245.48 14.50 -7 -1 0 244.38 13.80 -7 -1 0 239.88 15.70 7 -1 0 247.68 15.20 7 -1 0 251.07 14.40 7 -1 0 239.78 14.90 7 -1 0 238.28 15.50 -7 -1 0 225.28 15.30 7 -1 0 239.88 14.50 7 1 0 258.67 14.50 7 1 0 229.78 14.50 -7 1 0 238.58 14.40 7 1 0 235.08 15.60 -7 1 0 243.88 15.70 7 1 0 248.88 14.90 -7 1 0 252.67 14.40 -9 -1 0 1.80 2.70 -9 -1 0 5.10 3.40 -9 -1 0 5.80 2.80 9 -1 0 5.40 3.40 9 -1 0 -2.10 3.90 9 -1 0 -4.50 2.70 9 -1 0 2.40 2.70 9 -1 0 0.50 3.50 -9 -1 0 4.00 4.10 9 1 0 -3.20 2.90 9 1 0 -1.30 3.40 9 1 0 2.30 4.10 -9 1 0 0.50 2.70 9 1 0 -0.50 2.50 9 1 0 -2.50 3.00 -9 1 0 2.80 2.90 -9 1 0 4.40 4.50 11 -1 0 29.70 6.00 -11 -1 0 27.00 5.00 11 -1 0 22.60 5.50 -11 -1 0 33.30 5.40 11 -1 0 26.10 4.90 -11 1 0 29.80 5.10 11 1 0 31.30 9.60 11 1 0 22.80 5.90 11 1 0 30.40 5.70 11 1 0 25.40 5.10 -11 1 0 38.40 5.90 13 -1 0 12.70 6.10 -13 -1 0 17.70 6.40 13 -1 0 13.90 5.90 -13 -1 0 12.90 4.90 13 1 0 15.10 5.80 13 1 0 12.30 4.80 -13 1 0 20.80 5.30 13 1 0 10.70 5.20 -13 1 0 22.10 5.90 -15 -1 0 -8.60 4.50 15 -1 0 -2.10 7.30 15 -1 0 4.10 6.00 15 1 0 -5.70 5.30 -15 1 0 0.20 5.20 15 1 0 -0.10 5.90 17 -1 0 16.90 9.00 17 -1 0 19.20 8.90 -17 -1 0 9.20 7.10 17 1 0 6.30 9.60 -17 1 0 17.80 7.30 17 1 0 9.50 7.70 19 -1 0 22.50 10.40 -19 -1 0 7.40 9.10 19 -1 0 11.00 9.80 -19 1 0 7.20 9.00 19 1 0 12.10 9.00 19 1 0 10.00 11.80 2 -2 0 811.52 42.20 -2 -2 0 783.82 42.30 -2 -2 0 804.12 42.10 2 -2 0 808.52 43.60 -2 -2 0 819.92 42.20 2 -2 0 807.52 41.80 -2 -2 0 799.72 42.20 2 -2 0 787.02 42.00 -2 2 0 824.02 42.20 -2 2 0 799.92 41.90 -2 2 0 774.62 42.00 2 2 0 828.22 42.10 2 2 0 810.62 42.30 2 2 0 783.62 42.20 -2 2 0 810.62 42.20 -4 -2 0 4959.00 252.77 -4 -2 0 5017.40 252.07 -4 -2 0 4772.12 252.07 -4 -2 0 4750.32 252.27 4 -2 0 4727.53 252.57 4 -2 0 5068.09 252.07 -4 -2 0 5072.09 252.27 4 -2 0 4679.63 252.37 4 2 0 4930.81 252.27 4 2 0 4675.23 252.67 -4 2 0 4986.20 251.97 -4 2 0 4991.60 252.67 4 2 0 4745.93 252.17 -4 2 0 4882.51 251.97 -4 2 0 4908.81 252.47 -6 -2 0 485.25 26.30 -6 -2 0 496.25 25.90 -6 -2 0 486.55 27.20 6 -2 0 453.45 26.60 6 -2 0 480.15 26.00 6 -2 0 477.95 26.10 6 -2 0 496.25 26.70 6 -2 0 467.95 26.90 -6 -2 0 465.75 26.10 -6 -2 0 446.66 26.40 -6 2 0 492.75 27.10 6 2 0 487.55 26.50 6 2 0 491.35 26.20 6 2 0 455.55 27.10 -6 2 0 466.85 26.00 -6 2 0 481.55 26.00 6 2 0 459.05 26.20 -8 -2 0 1236.28 65.69 -8 -2 0 1273.37 65.39 -8 -2 0 1205.08 67.09 -8 -2 0 1245.18 65.89 8 -2 0 1238.28 66.79 8 -2 0 1211.08 66.49 8 -2 0 1255.57 66.39 -8 -2 0 1182.78 66.19 8 -2 0 1276.67 65.69 -8 2 0 1230.38 65.59 -8 2 0 1227.68 67.09 8 2 0 1266.77 66.19 8 2 0 1208.98 65.89 8 2 0 1201.28 66.89 8 2 0 1264.07 65.79 -8 2 0 1274.37 65.59 -10 -2 0 36.80 5.40 10 -2 0 38.90 5.50 -10 -2 0 26.00 6.60 10 -2 0 46.30 6.80 10 -2 0 35.00 5.90 10 -2 0 30.60 5.60 -10 -2 0 43.00 6.30 -10 -2 0 36.10 5.40 -10 2 0 43.00 6.00 10 2 0 46.30 6.70 10 2 0 35.70 6.70 10 2 0 46.10 6.80 10 2 0 30.80 5.20 -10 2 0 25.80 6.30 -10 2 0 51.19 6.10 10 2 0 35.50 5.60 -12 -2 0 148.49 11.90 12 -2 0 157.88 13.30 -12 -2 0 147.79 12.90 12 -2 0 173.68 14.20 -12 2 0 167.98 12.10 12 2 0 143.79 12.00 -12 2 0 162.78 12.50 12 2 0 176.38 14.50 12 2 0 152.88 13.00 14 -2 0 14.90 6.70 -14 -2 0 19.20 5.50 14 -2 0 12.30 7.20 -14 2 0 14.60 6.50 14 2 0 18.10 6.50 -14 2 0 15.00 5.50 14 2 0 13.40 6.20 14 2 0 15.70 5.10 -16 -2 0 0.80 5.70 16 -2 0 0.70 7.20 16 -2 0 4.60 6.80 -16 2 0 4.40 6.10 16 2 0 -11.30 7.10 16 2 0 5.70 7.00 18 -2 0 10.50 9.40 -18 -2 0 14.10 8.00 18 -2 0 17.80 9.00 18 2 0 9.50 9.60 18 2 0 3.40 8.50 -18 2 0 19.60 8.20 20 -2 0 -4.00 10.50 20 -2 0 2.60 10.80 -20 -2 0 13.70 10.00 20 2 0 -2.30 10.10 20 2 0 6.40 12.80 1 -3 0 1595.64 83.99 1 -3 0 1593.44 84.39 1 -3 0 1656.33 84.49 -1 -3 0 1670.83 84.49 -1 -3 0 1643.44 84.39 -1 -3 0 1596.34 84.19 1 -3 0 1567.94 84.19 -1 3 0 1677.03 83.99 -1 3 0 1573.04 84.39 -1 3 0 1598.04 84.39 -1 3 0 1678.83 84.49 1 3 0 1591.64 84.19 1 3 0 1616.34 84.79 3 -3 0 2792.52 144.39 3 -3 0 2744.93 144.49 3 -3 0 2750.42 143.89 -3 -3 0 2734.83 144.59 3 -3 0 2849.51 144.19 -3 -3 0 2673.93 144.29 -3 -3 0 2898.31 144.49 -3 -3 0 2808.92 144.39 -3 3 0 2815.52 144.49 -3 3 0 2756.22 144.09 3 3 0 2780.12 144.69 -3 3 0 2841.12 144.49 3 3 0 2857.01 144.29 3 3 0 2764.12 144.39 -3 3 0 2669.73 144.19 -5 -3 0 32.70 4.60 -5 -3 0 16.50 2.90 5 -3 0 22.70 3.30 -5 -3 0 25.40 3.60 5 -3 0 17.50 3.10 5 -3 0 22.10 3.60 -5 -3 0 24.10 3.50 -5 -3 0 22.30 3.10 5 3 0 21.70 3.30 5 3 0 18.50 3.20 -5 3 0 25.90 3.90 -5 3 0 22.10 3.10 -5 3 0 25.70 3.70 -5 3 0 20.40 2.90 5 3 0 24.30 3.30 7 -3 0 1231.08 65.49 7 -3 0 1200.88 65.49 7 -3 0 1239.08 65.89 -7 -3 0 1206.58 64.89 7 -3 0 1271.57 64.89 -7 -3 0 1205.98 65.39 -7 -3 0 1222.18 65.19 -7 -3 0 1200.98 66.09 -7 -3 0 1242.78 64.89 -7 3 0 1277.37 64.79 -7 3 0 1211.88 64.79 -7 3 0 1234.38 65.99 7 3 0 1192.28 65.09 7 3 0 1247.48 65.29 7 3 0 1194.88 66.09 9 -3 0 30.30 5.30 9 -3 0 42.30 5.40 9 -3 0 32.90 5.60 -9 -3 0 36.90 5.40 9 -3 0 38.40 6.00 -9 -3 0 39.40 5.90 -9 -3 0 41.40 7.40 -9 -3 0 39.20 7.00 -9 -3 0 36.90 5.40 9 3 0 33.20 6.00 9 3 0 36.20 5.60 -9 3 0 34.20 6.70 -9 3 0 36.80 5.50 9 3 0 33.90 5.10 -9 3 0 42.90 5.30 -11 -3 0 310.17 20.20 11 -3 0 339.17 21.50 11 -3 0 330.97 20.90 -11 -3 0 319.07 20.80 -11 -3 0 320.17 19.60 -11 -3 0 306.57 19.80 -11 3 0 323.67 19.60 11 3 0 326.17 20.00 -11 3 0 304.67 19.40 11 3 0 329.87 21.70 13 -3 0 125.49 12.10 -13 -3 0 97.69 13.10 -13 -3 0 110.19 10.40 13 -3 0 100.89 12.00 13 3 0 112.29 10.50 13 3 0 100.99 12.50 -13 3 0 118.09 10.40 -13 3 0 101.49 11.20 13 3 0 106.89 11.60 15 -3 0 4.20 6.10 -15 -3 0 5.50 5.50 15 -3 0 1.30 6.00 15 3 0 10.30 7.80 -15 3 0 -4.90 5.00 15 3 0 4.20 6.10 -15 3 0 1.20 8.30 15 3 0 -1.00 4.70 17 -3 0 65.49 11.80 17 -3 0 53.89 10.60 -17 -3 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189.88 14.00 -9 7 0 219.28 16.40 11 -7 0 351.26 23.50 -11 -7 0 363.26 24.00 -11 -7 0 383.46 22.60 11 -7 0 360.96 23.50 -11 -7 0 362.96 23.20 11 7 0 386.36 24.70 11 7 0 359.86 22.80 -11 7 0 343.87 21.60 -11 7 0 360.06 22.30 -13 -7 0 41.40 7.10 -13 -7 0 36.90 9.90 13 -7 0 28.30 7.50 -13 -7 0 44.60 8.30 13 -7 0 36.20 7.60 13 7 0 21.00 9.00 13 7 0 29.00 6.60 -13 7 0 34.00 7.00 -13 7 0 30.50 7.00 -15 -7 0 160.68 14.40 15 -7 0 148.29 15.80 15 -7 0 158.08 16.50 15 7 0 163.88 16.00 -15 7 0 160.28 14.50 15 7 0 155.68 17.70 15 7 0 151.78 14.60 -17 -7 0 -7.10 7.00 17 -7 0 -6.90 8.50 -17 7 0 3.40 8.80 17 7 0 -4.30 10.90 17 7 0 7.60 7.20 17 7 0 6.40 8.80 19 -7 0 3.80 11.40 19 -7 0 17.80 11.50 -19 -7 0 6.10 8.80 19 7 0 -4.70 12.40 19 7 0 12.40 9.10 19 7 0 18.90 11.20 -19 7 0 11.90 12.20 0 -8 0 590.84 34.60 0 -8 0 614.44 33.90 0 -8 0 614.64 33.90 0 8 0 563.24 33.50 0 8 0 611.54 34.00 0 8 0 592.44 33.50 2 -8 0 364.56 21.00 2 -8 0 365.76 22.80 2 -8 0 398.46 22.70 -2 -8 0 370.26 22.30 2 -8 0 387.16 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8.90 3 -15 0 10.20 6.20 -3 -15 0 15.30 6.40 3 -15 0 -11.90 7.70 3 15 0 3.00 4.80 -3 15 0 9.90 4.50 3 15 0 0.10 4.60 3 15 0 9.10 7.60 -3 15 0 5.00 5.00 -3 15 0 8.30 8.90 5 -15 0 84.79 11.50 5 -15 0 65.39 11.00 -5 -15 0 82.59 11.70 5 15 0 77.59 10.70 -5 15 0 90.89 10.00 5 15 0 70.19 10.00 5 15 0 73.09 11.60 -5 15 0 80.89 11.60 7 -15 0 88.49 12.70 7 -15 0 73.79 11.40 7 -15 0 72.09 11.50 -7 -15 0 95.99 13.40 7 15 0 87.99 12.00 -7 15 0 115.69 13.40 7 15 0 80.69 11.00 -7 15 0 93.69 12.60 9 -15 0 25.80 8.60 9 -15 0 23.40 8.70 -9 -15 0 25.50 9.00 9 -15 0 17.50 11.00 -9 15 0 30.10 8.90 -9 15 0 21.00 7.60 9 15 0 11.60 7.40 9 15 0 22.50 8.50 -9 15 0 48.10 10.40 11 -15 0 148.89 15.40 11 -15 0 135.99 16.00 -11 -15 0 150.58 17.20 -11 -15 0 124.69 14.70 -11 15 0 150.18 17.80 11 15 0 116.89 15.10 11 15 0 135.09 16.20 13 -15 0 -5.20 8.40 -13 -15 0 -2.40 7.40 -13 -15 0 5.40 9.90 13 -15 0 -0.30 8.00 13 15 0 -5.70 11.60 -13 15 0 -17.20 9.90 13 15 0 -2.60 11.20 -15 -15 0 82.09 17.50 -15 -15 0 90.79 13.20 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25.60 5 -3 4 1917.01 109.89 -5 -3 -4 2058.59 107.99 5 -3 4 2012.40 108.19 -5 -3 -4 1972.50 107.49 5 -3 4 2093.89 107.89 -5 -3 -4 2103.19 107.69 5 -3 4 2126.89 107.69 5 3 4 2035.70 107.09 5 3 4 1785.82 108.09 -5 3 -4 2126.79 107.99 5 3 4 2091.19 108.29 -5 3 -4 2170.58 108.79 5 3 4 2205.08 108.09 -5 3 -4 2087.99 107.49 -7 3 -4 42.70 5.60 7 3 4 38.50 5.20 7 3 4 38.80 5.00 -7 3 -4 41.40 5.70 7 3 4 45.00 6.10 7 3 4 47.30 6.40 -7 3 -4 40.60 6.00 -7 3 -4 45.80 5.50 -7 3 -4 42.30 5.00 -9 -3 -4 438.96 25.60 9 -3 4 447.06 26.80 -9 -3 -4 431.36 25.30 -9 -3 -4 415.56 26.60 9 -3 4 420.76 25.30 -9 -3 -4 421.56 26.00 9 -3 4 437.46 26.00 9 -3 4 455.05 26.40 -9 3 -4 462.35 25.60 -9 3 -4 416.26 26.90 9 3 4 427.96 25.90 9 3 4 435.06 26.60 -9 3 -4 444.36 25.50 -9 3 -4 433.76 24.40 9 3 4 418.46 25.20 9 3 4 450.95 25.50 -11 -3 -4 169.38 12.70 -11 -3 -4 158.38 11.40 11 -3 4 164.68 13.50 11 3 4 127.89 11.00 11 3 4 112.39 12.30 -11 3 -4 125.79 9.70 -11 3 -4 126.89 11.20 11 3 4 123.49 11.00 -11 3 -4 125.69 12.40 -13 -3 -4 60.39 8.90 13 -3 4 57.39 10.00 13 -3 4 61.49 9.30 -13 -3 -4 46.30 8.20 13 3 4 68.29 10.90 13 3 4 60.39 9.30 -13 3 -4 70.19 9.80 -13 3 -4 64.29 7.10 -15 -3 -4 93.29 11.90 15 -3 4 98.19 12.70 15 -3 4 93.99 13.70 15 3 4 76.59 11.00 15 3 4 90.19 14.30 -15 3 -4 87.49 12.40 17 -3 4 15.40 9.10 17 -3 4 23.80 9.30 -17 -3 -4 27.60 8.50 17 3 4 25.20 9.20 -17 3 -4 34.00 9.10 17 3 4 29.30 11.90 19 -3 4 47.00 12.70 19 -3 4 62.79 12.90 -19 -3 -4 52.69 11.20 -19 3 -4 60.29 11.90 19 3 4 37.00 11.80 19 3 4 48.40 13.00 -18 -4 4 38.60 8.60 18 -4 -4 56.59 12.90 18 -4 -4 40.60 10.60 18 4 -4 43.80 12.00 18 4 -4 25.80 11.30 16 -4 -4 -3.40 8.20 -16 -4 4 4.80 5.40 16 -4 -4 -4.00 6.40 16 4 -4 7.50 7.70 16 4 -4 1.60 7.70 16 4 -4 2.70 5.80 14 -4 -4 83.99 12.20 -14 -4 4 93.59 9.40 14 -4 -4 96.99 12.20 -14 -4 4 129.09 15.50 14 4 -4 79.39 12.00 14 4 -4 76.09 10.10 12 -4 -4 27.50 6.10 -12 -4 4 35.30 5.50 -12 -4 4 20.30 7.00 12 -4 -4 30.20 6.40 12 4 -4 23.90 5.50 12 4 -4 38.90 8.50 10 -4 -4 206.98 15.40 -10 -4 4 207.88 13.80 -10 -4 4 218.18 13.90 10 -4 -4 225.58 15.70 -10 -4 4 221.28 15.60 10 -4 -4 207.68 13.80 10 -4 -4 220.88 15.50 -10 4 4 234.48 18.20 10 4 -4 216.48 14.60 10 4 -4 225.28 16.90 10 4 -4 223.68 14.70 8 -4 -4 304.77 24.60 8 -4 -4 335.57 18.20 -8 -4 4 322.47 19.80 8 -4 -4 315.87 19.70 -8 -4 4 314.07 18.80 8 -4 -4 321.97 18.10 8 -4 -4 324.27 19.80 -8 -4 4 322.37 18.40 8 4 -4 312.57 18.60 8 4 -4 301.37 21.00 8 4 -4 310.87 19.20 -8 4 4 319.17 20.70 -6 -4 4 573.74 31.50 -6 -4 4 571.34 32.30 -6 -4 4 596.94 31.70 6 -4 -4 598.84 31.10 6 -4 -4 586.24 32.50 6 -4 -4 509.05 31.50 -6 -4 4 613.94 33.20 6 -4 -4 597.54 36.50 6 -4 -4 563.74 32.30 6 4 -4 601.34 34.00 6 4 -4 603.14 32.50 6 4 -4 570.84 32.10 6 4 -4 599.54 32.80 4 -4 -4 1235.58 64.79 -4 -4 4 1181.18 66.79 4 -4 -4 1240.68 65.79 4 -4 -4 1281.47 68.69 4 -4 -4 1269.77 65.69 -4 -4 4 1246.38 66.39 -4 -4 4 1252.17 64.99 4 4 -4 1259.17 66.59 4 4 -4 1202.58 66.29 4 4 -4 1276.97 64.99 -2 -4 4 839.12 44.80 2 -4 -4 804.32 46.40 -2 -4 4 852.81 44.90 2 -4 -4 822.82 44.10 2 -4 -4 812.22 44.00 2 4 -4 872.11 45.20 -2 4 4 817.12 47.10 2 4 -4 849.72 46.10 2 4 -4 845.22 45.30 0 -4 4 1525.85 77.19 0 -4 -4 1445.06 75.89 0 -4 4 1463.65 78.49 0 -4 -4 1464.95 75.99 0 -4 4 1491.55 76.89 0 -4 -4 1453.25 76.19 0 -4 -4 1448.85 77.19 0 4 4 1410.76 78.69 0 4 -4 1453.05 77.39 0 4 -4 1419.76 77.09 0 4 -4 1555.34 78.39 0 4 -4 1448.16 77.09 -2 -4 -4 839.92 43.10 -2 -4 -4 808.32 43.70 2 -4 4 860.21 43.90 2 -4 4 815.42 45.40 2 -4 4 801.82 44.10 -2 -4 -4 882.61 43.20 -2 4 -4 802.72 43.60 -2 4 -4 788.72 47.70 2 4 4 833.02 43.50 2 4 4 755.32 42.90 -2 4 -4 769.72 43.60 4 -4 4 1079.49 63.29 -4 -4 -4 1211.78 62.89 4 -4 4 1162.68 63.79 -4 -4 -4 1128.69 63.29 4 -4 4 1157.28 63.99 4 -4 4 1205.08 62.99 4 -4 4 1198.78 63.09 -4 -4 -4 1203.48 62.89 4 4 4 1211.88 63.29 4 4 4 1178.18 62.79 -4 4 -4 1230.38 63.59 -4 4 -4 1168.78 62.89 -4 4 -4 1221.28 63.19 -4 4 -4 1204.28 64.09 4 4 4 1281.07 63.39 -6 -4 -4 592.94 32.50 6 -4 4 598.44 32.40 6 -4 4 609.34 32.00 -6 -4 -4 608.54 32.00 -6 -4 -4 598.94 32.40 6 -4 4 572.64 32.70 -6 -4 -4 574.84 31.90 6 4 4 555.74 31.30 -6 4 -4 570.24 32.30 -6 4 -4 541.55 32.00 -6 4 -4 563.14 33.10 6 4 4 557.64 31.80 6 4 4 596.64 32.40 -6 4 -4 546.85 31.50 8 -4 4 291.17 18.90 -8 -4 -4 300.67 19.20 8 -4 4 272.47 18.00 8 -4 4 303.87 19.60 -8 -4 -4 293.07 18.30 -8 -4 -4 290.67 18.10 -8 -4 -4 272.87 18.70 8 -4 4 290.17 18.80 -8 4 -4 290.57 17.40 8 4 4 284.37 18.80 8 4 4 305.77 19.30 -8 4 -4 323.87 18.50 -8 4 -4 309.07 18.80 8 4 4 313.47 18.30 -8 4 -4 297.87 19.90 -8 4 -4 308.17 18.20 8 4 4 311.67 18.90 10 -4 4 238.08 15.70 10 -4 4 219.58 16.40 -10 -4 -4 249.48 19.40 -10 -4 -4 205.98 15.70 -10 -4 -4 222.58 14.80 10 4 4 193.38 14.50 -10 4 -4 203.78 13.50 -10 4 -4 189.38 14.90 10 4 4 217.08 14.50 -10 4 -4 226.28 14.90 10 4 4 223.68 16.20 -12 -4 -4 24.30 5.90 -12 -4 -4 33.20 6.80 12 -4 4 44.20 7.50 12 -4 4 25.90 7.50 -12 4 -4 32.70 6.60 12 4 4 36.70 9.00 12 4 4 42.40 6.90 -12 4 -4 33.20 5.00 12 4 4 38.50 6.40 14 -4 4 86.39 12.20 -14 -4 -4 82.29 10.80 14 -4 4 77.99 11.90 -14 -4 -4 81.79 12.20 -14 -4 -4 81.59 10.50 14 4 4 89.29 13.10 14 4 4 84.09 10.80 -14 4 -4 77.89 10.90 16 -4 4 -9.00 7.20 16 -4 4 -10.70 7.30 -16 -4 -4 -12.50 6.00 16 4 4 8.30 8.70 -16 4 -4 4.80 7.10 16 4 4 6.50 7.40 18 -4 4 52.19 13.80 18 -4 4 32.10 10.90 -18 -4 -4 46.10 10.20 18 4 4 38.50 12.70 18 4 4 63.49 18.00 -18 4 -4 59.79 11.20 -19 -5 4 18.00 9.10 19 -5 -4 12.90 10.30 19 -5 -4 7.90 10.00 19 5 -4 36.00 13.80 19 5 -4 22.30 11.40 19 5 -4 24.80 9.20 17 -5 -4 17.30 8.50 -17 -5 4 11.30 6.60 17 5 -4 10.40 8.40 17 5 -4 -0.30 6.70 17 5 -4 5.30 9.90 15 -5 -4 67.39 11.40 -15 -5 4 65.49 9.70 15 -5 -4 83.19 12.00 15 5 -4 103.39 15.20 15 5 -4 68.69 9.80 -13 -5 4 106.69 14.50 13 -5 -4 101.89 11.90 -13 -5 4 112.89 9.90 13 -5 -4 123.09 12.50 13 5 -4 104.49 13.70 13 5 -4 84.79 10.40 -11 -5 4 115.79 13.10 -11 -5 4 137.69 11.00 -11 -5 4 136.19 10.60 11 -5 -4 142.49 11.10 11 -5 -4 137.49 12.60 11 -5 -4 141.19 12.70 11 5 -4 145.69 12.10 11 5 -4 153.98 14.10 11 5 -4 161.88 11.80 9 -5 -4 820.02 44.80 9 -5 -4 837.72 45.00 9 -5 -4 818.02 43.20 9 -5 -4 763.22 49.70 -9 -5 4 795.42 44.90 -9 -5 4 819.02 43.50 -9 -5 4 807.32 44.10 -9 -5 4 823.52 44.10 9 5 -4 794.32 43.80 -9 5 4 748.63 45.70 9 5 -4 809.52 46.40 9 5 -4 777.42 44.20 -7 -5 4 58.09 6.20 -7 -5 4 66.29 8.40 -7 -5 4 55.49 7.10 7 -5 -4 64.79 7.00 7 -5 -4 59.49 5.50 7 -5 -4 63.79 11.40 7 -5 -4 68.69 6.90 -7 -5 4 56.69 6.40 7 5 -4 79.69 8.80 -7 5 4 79.79 8.40 7 5 -4 74.69 7.30 7 5 -4 75.49 7.70 7 5 -4 80.19 6.30 -5 -5 4 1465.15 74.39 5 -5 -4 1391.86 76.79 -5 -5 4 1284.37 75.59 -5 -5 4 1383.76 72.99 5 -5 -4 1429.56 72.79 5 -5 -4 1319.67 73.99 5 -5 -4 1376.96 73.49 5 5 -4 1402.36 74.29 5 5 -4 1442.06 72.99 5 5 -4 1408.06 75.59 5 5 -4 1413.56 74.69 -3 -5 4 83.39 8.00 3 -5 -4 104.79 10.10 -3 -5 4 86.29 5.90 3 -5 -4 89.29 6.30 3 -5 -4 86.89 6.60 3 -5 -4 86.89 6.50 -3 -5 4 88.19 7.60 3 5 -4 102.99 8.50 3 5 -4 111.19 6.10 3 5 -4 102.29 9.90 3 5 -4 100.79 8.30 -3 5 4 97.39 10.80 1 -5 -4 703.73 36.00 1 -5 -4 670.03 34.30 -1 -5 4 666.33 35.80 -1 -5 4 658.83 35.70 -1 -5 4 646.14 34.60 1 -5 -4 647.84 36.90 -1 -5 4 645.14 35.90 1 5 -4 631.14 36.00 -1 5 4 613.24 37.20 -1 5 4 667.93 34.50 1 5 -4 622.24 35.90 1 5 -4 652.43 36.50 1 5 -4 643.74 35.80 1 -5 4 641.84 37.60 -1 -5 -4 641.04 34.70 1 -5 4 626.34 35.60 -1 -5 -4 665.73 34.40 1 -5 4 667.73 35.70 -1 5 -4 650.03 35.80 -1 5 -4 686.63 37.40 1 5 4 672.13 35.60 1 5 4 636.24 34.50 -1 5 -4 649.83 35.70 -3 -5 -4 102.89 6.60 -3 -5 -4 92.59 7.30 3 -5 4 93.79 8.50 -3 -5 -4 99.39 6.70 3 -5 4 98.39 7.10 3 5 4 88.59 6.80 -3 5 -4 82.09 8.00 3 5 4 82.49 6.40 -3 5 -4 85.59 7.00 -3 5 -4 82.19 7.00 3 5 4 89.89 7.10 -3 5 -4 80.99 8.30 5 -5 4 1444.16 72.69 -5 -5 -4 1364.56 72.89 5 -5 4 1412.46 73.09 5 -5 4 1353.26 73.89 -5 -5 -4 1385.06 72.79 5 -5 4 1346.77 73.69 -5 -5 -4 1393.96 72.79 5 -5 4 1400.26 72.89 -5 5 -4 1285.67 72.59 -5 5 -4 1347.57 72.99 5 5 4 1329.27 72.59 -5 5 -4 1403.96 74.09 5 5 4 1429.96 73.19 5 5 4 1369.16 73.19 -5 5 -4 1358.66 73.39 -7 -5 -4 68.59 7.60 7 -5 4 79.39 7.80 -7 -5 -4 78.49 7.30 7 -5 4 68.39 6.90 7 -5 4 70.59 7.70 -7 -5 -4 77.19 7.00 7 -5 4 67.19 8.00 -7 -5 -4 77.89 8.00 7 5 4 61.59 7.10 7 5 4 50.19 6.20 -7 5 -4 55.59 6.10 -7 5 -4 52.59 7.70 -7 5 -4 62.99 7.00 7 5 4 50.09 7.30 -7 5 -4 59.49 7.30 -9 -5 -4 766.12 43.10 -9 -5 -4 746.83 42.60 -9 -5 -4 753.92 43.50 9 -5 4 776.42 43.70 9 -5 4 691.73 42.90 9 -5 4 747.43 42.30 -9 -5 -4 781.02 42.40 9 -5 4 762.02 43.20 9 5 4 823.72 42.10 -9 5 -4 806.22 42.60 -9 5 -4 759.12 41.40 -9 5 -4 725.03 42.90 -9 5 -4 771.52 42.30 9 5 4 776.12 42.40 9 5 4 766.42 43.60 -9 5 -4 745.13 44.10 9 5 4 780.52 43.10 11 -5 4 158.18 12.90 -11 -5 -4 156.28 12.90 11 -5 4 167.38 13.80 -11 -5 -4 164.08 11.90 -11 5 -4 120.59 11.60 -11 5 -4 123.69 12.70 11 5 4 131.49 11.40 -11 5 -4 123.39 10.20 11 5 4 116.59 12.90 11 5 4 130.89 11.20 13 -5 4 101.29 13.10 13 -5 4 92.49 12.10 -13 -5 -4 99.79 12.40 -13 -5 -4 99.29 11.00 -13 -5 -4 82.99 12.30 13 5 4 104.39 11.00 13 5 4 108.89 11.20 -13 5 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99.29 9.50 -10 -6 4 109.79 10.10 -10 6 4 103.09 13.60 10 6 -4 103.89 11.80 10 6 -4 98.69 9.30 10 6 -4 96.19 9.40 -8 -6 4 286.17 17.80 -8 -6 4 275.17 16.60 -8 -6 4 284.87 17.00 8 -6 -4 263.77 22.80 8 -6 -4 289.97 17.50 8 -6 -4 282.47 16.10 -8 -6 4 258.97 18.50 8 -6 -4 280.97 17.80 8 6 -4 255.77 19.10 8 6 -4 264.17 17.50 8 6 -4 276.27 16.50 -8 6 4 272.47 18.60 8 6 -4 238.28 18.60 6 -6 -4 16.30 3.00 6 -6 -4 15.70 6.70 -6 -6 4 13.30 3.20 -6 -6 4 18.90 5.10 6 -6 -4 13.60 3.50 6 -6 -4 20.20 4.20 -6 -6 4 18.30 4.90 6 6 -4 7.10 4.20 6 6 -4 11.40 4.50 -6 6 4 8.90 4.10 6 6 -4 7.50 2.80 6 6 -4 14.70 4.20 -4 -6 4 1550.24 84.49 -4 -6 4 1537.35 82.59 4 -6 -4 1607.44 83.49 -4 -6 4 1650.43 84.49 4 -6 -4 1569.64 85.89 4 -6 -4 1600.54 82.89 4 -6 -4 1606.84 82.99 4 6 -4 1505.25 84.29 4 6 -4 1578.04 84.69 4 6 -4 1626.14 82.69 -2 -6 4 55.29 4.90 2 -6 -4 56.19 4.70 -2 -6 4 52.79 6.50 -2 -6 4 48.40 6.00 2 -6 -4 47.40 4.60 -2 6 4 51.59 8.40 2 6 -4 52.39 6.70 2 6 -4 54.89 7.00 2 6 -4 47.80 6.70 2 6 -4 62.79 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14 -10 4 21.20 8.40 -14 -10 -4 25.10 7.60 -14 10 -4 33.30 9.00 14 10 4 32.20 7.90 14 10 4 33.70 8.20 14 10 4 29.30 10.80 16 -10 4 132.79 18.70 -16 -10 -4 136.49 18.70 -16 -10 -4 138.39 16.00 16 -10 4 147.09 22.00 16 10 4 137.19 16.70 16 10 4 151.58 16.70 -16 10 -4 142.49 19.20 18 -10 4 17.50 13.80 18 -10 4 12.90 11.70 -18 -10 -4 14.70 10.30 18 10 4 37.60 14.80 -18 10 -4 19.70 14.10 18 10 4 14.20 11.10 -17 -11 4 30.10 9.20 17 -11 -4 17.90 10.30 17 -11 -4 38.40 11.20 17 11 -4 11.00 9.10 17 11 -4 -2.70 11.60 15 -11 -4 -2.90 10.30 15 -11 -4 0.60 8.30 -15 -11 4 5.20 7.00 15 11 -4 6.50 12.50 15 11 -4 5.10 6.90 13 -11 -4 25.50 8.10 -13 -11 4 14.60 7.30 -13 -11 4 19.60 6.60 13 -11 -4 5.30 6.70 13 11 -4 18.50 7.50 13 11 -4 15.10 10.80 -11 -11 4 20.10 5.80 11 -11 -4 17.60 6.10 -11 -11 4 12.30 5.90 11 -11 -4 20.00 7.10 11 11 -4 23.70 8.90 11 11 -4 25.40 7.20 9 -11 -4 -5.00 11.50 9 -11 -4 0.80 4.40 -9 -11 4 -3.90 4.40 -9 -11 4 0.80 4.80 9 -11 -4 -0.40 4.70 9 11 -4 7.70 5.30 -9 11 4 6.60 7.10 9 11 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192.08 19.30 16 12 -4 171.38 26.40 -14 -12 4 -6.60 6.50 14 -12 -4 9.20 8.00 -14 -12 4 10.80 8.10 14 -12 -4 -3.70 7.00 14 12 -4 4.90 7.40 14 12 -4 2.20 11.60 12 -12 -4 106.39 12.40 12 -12 -4 113.89 13.80 -12 -12 4 94.59 11.70 -12 -12 4 102.19 13.00 12 12 -4 112.39 15.40 12 12 -4 103.59 13.50 -10 -12 4 11.30 5.90 10 -12 -4 14.30 5.40 -10 -12 4 9.30 5.80 10 -12 -4 14.80 6.20 10 12 -4 9.00 7.50 10 12 -4 6.50 6.10 10 12 -4 13.60 7.20 -10 12 4 31.20 10.10 8 -12 -4 15.90 10.60 8 -12 -4 5.80 4.90 8 -12 -4 11.40 4.80 8 -12 -4 21.60 6.20 -8 -12 4 11.30 5.10 8 -12 -4 0.60 7.00 8 12 -4 6.90 5.60 8 12 -4 17.10 7.00 8 12 -4 11.20 5.50 -8 12 4 13.20 6.40 6 -12 -4 22.30 8.20 6 -12 -4 19.30 5.80 6 -12 -4 21.10 6.70 -6 -12 4 26.00 5.80 -6 -12 4 18.60 8.30 6 -12 -4 29.90 7.20 6 -12 -4 16.50 4.00 6 12 -4 25.30 7.00 6 12 -4 25.40 7.10 -6 12 4 15.80 6.00 6 12 -4 18.00 6.50 4 -12 -4 463.25 27.10 -4 -12 4 477.25 26.40 4 -12 -4 460.85 26.80 4 -12 -4 469.55 27.90 4 -12 -4 456.65 27.10 -4 -12 4 418.16 28.40 -4 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7.30 3 13 4 5.20 3.90 -3 13 -4 11.60 6.50 3 13 4 7.90 4.90 -3 13 -4 11.00 6.20 -3 13 -4 8.20 5.90 5 -13 4 107.09 14.00 -5 -13 -4 127.69 13.10 5 -13 4 124.99 13.60 -5 13 -4 128.39 12.90 -5 13 -4 113.09 12.90 5 13 4 112.39 10.50 5 13 4 113.89 12.10 5 13 4 116.69 10.10 -5 13 -4 105.69 13.70 -7 -13 -4 1.20 6.10 7 -13 4 -5.00 6.60 7 -13 4 -4.20 6.00 -7 13 -4 4.30 5.90 7 13 4 3.60 4.80 -7 13 -4 29.20 9.10 7 13 4 1.70 6.10 -7 13 -4 -5.30 5.30 7 13 4 -0.90 4.30 9 -13 4 61.39 10.70 -9 -13 -4 75.89 10.80 9 -13 4 75.79 10.10 -9 -13 -4 75.79 10.30 9 13 4 84.79 10.70 -9 13 -4 79.79 12.10 -9 13 -4 92.79 13.10 9 13 4 75.79 11.40 9 13 4 87.19 12.90 -11 -13 -4 14.80 8.10 -11 -13 -4 11.10 6.20 11 -13 4 5.10 7.70 11 13 4 11.30 7.80 -11 13 -4 12.80 7.40 11 13 4 8.10 6.40 -11 13 -4 13.00 8.70 -13 -13 -4 33.60 8.30 -13 -13 -4 66.79 12.60 13 -13 4 30.50 9.90 13 -13 4 26.10 9.60 -13 13 -4 42.80 8.00 13 13 4 22.60 10.70 -13 13 -4 22.80 10.50 13 13 4 39.20 9.30 15 -13 4 2.90 10.40 15 -13 4 5.10 10.40 -15 -13 -4 16.70 9.20 -15 -13 -4 1.50 7.90 -15 13 -4 -11.00 12.00 15 13 4 3.00 8.30 15 13 4 3.10 8.40 15 13 4 -13.50 10.30 -17 -13 -4 0.80 12.50 -17 -13 -4 -9.50 9.30 17 -13 4 4.00 13.20 17 -13 4 10.10 13.40 -17 13 -4 17.20 15.50 17 13 4 5.70 13.40 17 13 4 -11.80 11.20 17 13 4 7.20 10.40 -16 -14 4 50.19 11.20 16 -14 -4 69.39 14.50 16 -14 -4 63.59 14.00 16 14 -4 83.39 16.40 16 14 -4 79.39 13.60 14 -14 -4 23.70 10.00 14 -14 -4 10.20 8.60 -14 -14 4 0.90 9.10 -14 -14 4 0.40 7.40 14 14 -4 24.20 14.90 14 14 -4 6.90 8.70 12 -14 -4 10.70 7.20 -12 -14 4 13.30 8.00 12 -14 -4 11.40 8.10 -12 -14 4 27.50 8.20 12 14 -4 12.50 10.20 12 14 -4 29.00 8.20 -10 -14 4 -4.80 6.30 10 -14 -4 -2.40 5.30 10 -14 -4 -2.50 6.10 -10 -14 4 -1.30 6.30 -10 14 4 5.80 10.60 10 14 -4 9.30 9.20 10 14 -4 3.20 7.00 8 -14 -4 85.89 13.10 -8 -14 4 93.09 11.30 8 -14 -4 87.79 10.10 8 -14 -4 99.29 14.60 8 -14 -4 104.09 12.10 -8 14 4 83.29 10.50 8 14 -4 106.69 14.40 8 14 -4 85.19 12.20 6 -14 -4 23.70 8.00 6 -14 -4 30.60 8.80 6 -14 -4 13.50 6.10 -6 -14 4 21.90 6.40 6 14 -4 12.70 6.30 6 14 -4 11.90 7.20 -6 14 4 14.40 3.40 6 14 -4 11.80 8.20 -4 -14 4 395.36 24.40 4 -14 -4 363.26 25.50 4 -14 -4 408.86 25.10 4 -14 -4 371.76 25.30 -4 14 4 391.46 24.30 -4 14 4 381.76 22.00 4 14 -4 363.36 23.10 4 14 -4 378.06 25.30 4 14 -4 371.36 25.60 -2 -14 4 4.30 5.30 2 -14 -4 8.20 5.90 2 -14 -4 15.20 7.50 2 -14 -4 7.20 5.70 2 -14 -4 11.20 7.40 -2 14 4 4.80 5.90 2 14 -4 -0.10 5.10 2 14 -4 3.40 6.10 -2 14 4 -5.30 4.80 -2 14 4 2.80 3.70 0 -14 4 980.40 51.49 0 -14 4 952.70 54.99 0 -14 -4 923.91 53.09 0 -14 -4 951.40 52.09 0 -14 -4 878.01 51.99 0 -14 -4 896.61 53.09 0 14 4 920.31 50.99 0 14 4 854.81 50.29 0 14 4 886.21 49.70 0 14 -4 920.21 52.49 0 14 -4 876.61 52.39 -2 -14 -4 -3.40 5.30 2 -14 4 -7.90 5.90 2 14 4 -0.80 3.90 2 14 4 -6.90 4.80 -2 14 -4 -1.60 6.20 -2 14 -4 -0.70 6.20 -2 14 -4 1.00 5.50 4 -14 4 374.06 27.60 -4 -14 -4 377.16 25.80 4 -14 4 381.26 27.30 -4 14 -4 356.16 24.80 -4 14 -4 393.36 25.80 4 14 4 370.16 23.40 -4 14 -4 376.86 25.50 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18.40 6.50 1 15 -4 8.20 6.10 -1 15 4 7.00 5.80 -1 15 4 6.60 6.20 -1 15 4 13.80 4.70 -1 -15 -4 7.20 7.10 1 -15 4 8.50 7.40 -1 15 -4 23.80 7.20 1 15 4 23.90 6.20 -1 15 -4 28.20 7.50 1 15 4 23.40 5.40 -1 15 -4 13.00 6.70 1 15 4 12.70 6.30 3 -15 4 108.89 14.30 -3 -15 -4 107.49 14.10 -3 15 -4 109.09 13.00 3 15 4 105.09 12.40 -3 15 -4 111.39 13.80 3 15 4 91.49 10.40 -3 15 -4 88.89 12.70 3 15 4 122.49 11.40 -5 -15 -4 23.60 8.00 5 -15 4 40.70 10.50 -5 15 -4 40.50 9.30 -5 15 -4 31.20 8.70 -5 15 -4 30.80 8.70 5 15 4 36.80 7.80 5 15 4 32.70 6.80 -7 -15 -4 93.99 14.10 7 -15 4 101.99 15.20 7 15 4 96.89 11.50 -7 15 -4 100.39 14.70 7 15 4 84.99 11.40 -7 15 -4 117.49 13.70 7 15 4 99.39 14.90 9 -15 4 107.99 14.50 -9 -15 -4 115.39 13.30 9 -15 4 109.29 16.10 -9 -15 -4 98.79 13.20 9 15 4 106.89 13.80 -9 15 -4 121.39 14.40 -9 15 -4 107.19 15.90 9 15 4 94.09 14.00 9 15 4 100.39 12.80 -11 -15 -4 10.90 7.40 -11 -15 -4 14.50 9.40 11 -15 4 10.40 8.70 -11 15 -4 5.20 7.60 -11 15 -4 -11.00 9.00 11 15 4 -11.00 7.30 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16 -4 3.30 7.40 10 16 4 -3.30 7.00 -12 -16 -4 18.40 15.90 -12 -16 -4 21.40 10.30 -12 16 -4 23.50 12.20 12 16 4 22.20 10.10 -12 16 -4 24.40 8.70 -14 -16 -4 -10.90 10.40 -14 -16 -4 -6.30 8.60 14 -16 4 -21.50 11.00 14 16 4 6.30 12.20 -14 16 -4 12.00 14.10 14 16 4 15.50 9.90 15 -17 -4 -9.30 11.10 15 -17 -4 37.80 13.10 -15 -17 4 5.10 10.30 15 17 -4 17.50 16.70 15 17 -4 5.80 11.50 -13 -17 4 103.79 14.40 -13 -17 4 83.69 13.30 13 -17 -4 79.29 12.90 13 -17 -4 122.89 18.00 13 17 -4 88.09 14.50 -11 -17 4 17.00 9.80 -11 -17 4 16.00 9.30 11 -17 -4 28.50 10.00 11 17 -4 14.60 9.10 11 17 -4 10.20 11.70 -9 -17 4 98.89 13.00 9 -17 -4 85.99 13.20 9 17 -4 115.69 16.30 9 17 -4 116.09 15.60 7 -17 -4 140.59 16.60 -7 -17 4 119.29 16.00 7 -17 -4 160.18 19.40 7 17 -4 127.89 16.50 7 17 -4 142.09 16.60 7 17 -4 136.29 15.70 -5 -17 4 9.30 7.90 5 -17 -4 9.40 8.00 5 17 -4 21.90 9.20 5 17 -4 1.40 6.60 -5 17 4 20.30 5.20 -3 -17 4 136.99 15.70 3 -17 -4 142.49 16.10 3 -17 -4 154.78 16.00 -3 17 4 152.98 12.10 3 17 -4 134.09 15.30 3 17 -4 142.69 14.90 1 -17 -4 63.39 10.30 -1 -17 4 56.29 9.30 1 -17 -4 34.60 9.10 -1 17 4 43.30 8.00 -1 17 4 38.30 8.80 1 17 -4 30.60 8.00 -1 17 4 40.70 6.90 1 17 -4 31.30 8.30 1 -17 4 43.80 8.90 1 -17 4 34.40 10.50 -1 -17 -4 40.00 10.20 1 17 4 52.99 8.90 -1 17 -4 34.40 8.60 -1 17 -4 47.40 9.90 1 17 4 39.60 7.20 1 17 4 50.29 8.80 -1 17 -4 43.30 9.50 -3 -17 -4 139.79 16.90 3 -17 4 144.39 17.40 -3 17 -4 99.89 12.70 -3 17 -4 146.79 15.80 3 17 4 145.09 13.90 3 17 4 130.59 14.10 3 17 4 129.99 12.60 -3 17 -4 131.69 15.20 5 -17 4 10.40 9.20 -5 -17 -4 22.30 9.30 5 17 4 26.90 7.10 5 17 4 18.30 8.00 -5 17 -4 10.80 9.10 -5 17 -4 -2.30 8.40 -5 17 -4 20.10 8.50 7 -17 4 137.79 18.50 -7 -17 -4 152.48 18.30 -7 17 -4 152.08 16.00 7 17 4 115.39 13.40 -7 17 -4 119.69 17.30 7 17 4 108.59 15.00 7 17 4 131.09 14.20 -9 -17 -4 109.89 14.70 -9 -17 -4 81.59 14.70 9 -17 4 94.99 15.20 9 17 4 104.29 14.30 -9 17 -4 103.39 14.90 9 17 4 105.09 14.20 -9 17 -4 99.79 14.90 11 -17 4 3.40 18.30 -11 -17 -4 18.00 11.70 -11 -17 -4 17.40 9.70 11 17 4 26.90 10.30 11 17 4 33.80 9.70 -11 17 -4 24.20 11.80 -11 17 -4 14.70 8.80 13 -17 4 95.69 16.90 -13 -17 -4 127.69 17.20 -13 -17 -4 91.19 13.50 13 17 4 104.29 14.50 -13 17 -4 102.39 17.40 13 17 4 104.29 15.30 -15 -17 -4 22.80 14.70 15 -17 4 23.30 15.10 -15 -17 -4 -5.80 10.70 15 17 4 -12.00 9.90 15 17 4 -13.80 13.90 -15 17 -4 14.60 16.50 15 17 4 4.90 11.40 -14 -18 4 12.70 10.80 -14 -18 4 5.90 14.30 14 -18 -4 4.70 12.40 14 18 -4 3.80 16.30 14 18 -4 -5.20 10.80 -12 -18 4 38.50 11.50 12 -18 -4 47.90 13.00 -12 -18 4 57.09 13.40 12 18 -4 71.59 13.50 12 18 -4 74.39 16.30 10 -18 -4 14.20 9.70 -10 -18 4 0.80 10.20 10 18 -4 14.70 9.70 10 18 -4 4.50 10.40 8 -18 -4 10.00 9.50 -8 -18 4 30.10 10.00 8 18 -4 24.60 10.60 8 18 -4 39.10 9.30 -6 -18 4 25.00 9.50 6 -18 -4 15.30 9.30 6 18 -4 17.80 9.00 6 18 -4 30.70 8.70 6 18 -4 21.20 10.30 -6 18 4 24.60 5.60 4 -18 -4 2.40 7.90 -4 -18 4 0.00 8.20 4 18 -4 5.40 8.80 -4 18 4 0.40 4.90 4 18 -4 -0.60 6.60 4 18 -4 5.90 6.70 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