# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared), status flag # data_shelx _shelx_title ' pe1475a in P2/n' _shelx_refln_list_code 4 _shelx_F_calc_maximum 357.82 _exptl_crystal_F_000 842.88 _reflns_d_resolution_high 0.7600 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y, -z' '-x, -y, -z' 'x-1/2, -y, z' _cell_length_a 15.1359 _cell_length_b 7.2035 _cell_length_c 9.9876 _cell_angle_alpha 90.000 _cell_angle_beta 110.361 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 42271.62 45837.33 415.46 o 8 0 0 15450.85 15481.03 227.66 o 10 0 0 1470.56 1448.18 70.43 o 12 0 0 12434.64 13617.94 302.27 o 14 0 0 156.22 239.37 136.56 o 16 0 0 9782.16 9517.40 548.33 o 18 0 0 481.86 326.36 369.69 o 2 1 0 12438.70 12015.82 105.99 o 3 1 0 7145.73 8145.67 80.29 o 4 1 0 2135.10 2145.12 40.07 o 5 1 0 6011.98 6779.39 77.40 o 6 1 0 3705.85 3191.28 56.73 o 7 1 0 69.80 83.46 25.06 o 8 1 0 262.30 182.53 29.11 o 9 1 0 27.79 58.88 28.74 o 10 1 0 1324.38 1255.22 54.84 o 11 1 0 403.67 432.24 53.47 o 12 1 0 247.47 240.66 44.04 o 13 1 0 351.44 308.35 67.83 o 14 1 0 2716.49 2868.53 183.38 o 15 1 0 1681.43 1793.50 162.72 o 16 1 0 1.12 49.25 126.20 o 17 1 0 22.60 64.82 133.76 o 18 1 0 966.11 1027.07 235.18 o 0 2 0 5526.94 5486.86 121.50 o 1 2 0 47.73 162.30 31.06 o 2 2 0 4013.30 3849.66 68.74 o 3 2 0 439.17 399.23 31.90 o 4 2 0 9657.33 9441.52 150.98 o 5 2 0 332.61 300.09 33.93 o 6 2 0 1130.30 1039.58 46.25 o 7 2 0 293.68 322.22 35.35 o 8 2 0 66254.92 67488.65 487.83 o 9 2 0 24.39 37.00 26.89 o 10 2 0 59.41 64.64 31.97 o 11 2 0 871.23 833.01 61.34 o 12 2 0 8835.97 8944.44 248.44 o 13 2 0 8.27 55.61 73.72 o 14 2 0 428.96 449.88 90.66 o 15 2 0 17.42 203.45 108.25 o 16 2 0 5390.44 5679.81 286.72 o 17 2 0 46.46 -60.64 156.07 o 18 2 0 669.18 966.38 316.03 o 0 3 0 194.51 267.89 55.29 o 1 3 0 93.09 90.18 40.44 o 2 3 0 891.01 768.90 45.37 o 3 3 0 2471.58 3014.32 80.16 o 4 3 0 24.74 29.12 32.94 o 5 3 0 5.11 53.53 31.50 o 6 3 0 9876.45 9365.14 145.83 o 7 3 0 2514.96 2406.92 74.63 o 8 3 0 832.25 782.89 42.39 o 9 3 0 1011.40 1038.42 56.85 o 10 3 0 4291.81 4133.20 131.26 o 11 3 0 419.66 409.48 88.12 o 12 3 0 88.21 15.36 82.97 o 13 3 0 76.64 207.62 94.92 o 14 3 0 1655.26 1735.16 147.70 o 15 3 0 753.14 916.59 169.81 o 16 3 0 6.03 -122.90 142.45 o 17 3 0 83.31 5.02 142.66 o 0 4 0 94035.08 94724.53 1300.75 o 1 4 0 1371.26 1340.68 72.38 o 2 4 0 260.09 220.75 32.75 o 3 4 0 662.75 646.63 66.68 o 4 4 0 24243.19 23657.03 331.08 o 5 4 0 1195.88 1118.62 71.31 o 6 4 0 5.04 4.11 39.39 o 7 4 0 886.34 871.28 63.65 o 8 4 0 6090.68 6261.66 166.05 o 9 4 0 198.61 237.75 64.28 o 10 4 0 1387.24 1333.44 90.77 o 11 4 0 1643.85 1722.06 135.44 o 12 4 0 10712.80 10255.76 315.62 o 13 4 0 88.06 238.90 100.90 o 14 4 0 76.88 146.89 121.27 o 15 4 0 34.72 62.59 133.46 o 16 4 0 4790.00 4835.14 325.80 o 0 5 0 1175.29 1330.79 136.34 o 1 5 0 701.19 584.32 53.45 o 2 5 0 9336.86 8787.74 184.31 o 3 5 0 3157.06 3260.50 133.13 o 4 5 0 39.11 71.21 41.09 o 5 5 0 2782.66 2708.94 111.46 o 6 5 0 3418.44 3281.88 129.46 o 7 5 0 333.28 417.30 73.17 o 8 5 0 186.23 205.55 76.33 o 9 5 0 98.02 115.89 70.31 o 10 5 0 35.79 -90.06 94.95 o 11 5 0 55.39 240.05 107.08 o 12 5 0 129.17 -3.95 106.02 o 13 5 0 23.35 224.46 115.03 o 14 5 0 1288.14 1073.04 173.46 o 15 5 0 1339.29 1277.87 198.95 o 0 6 0 281.77 185.66 97.73 o 1 6 0 1208.21 1035.57 84.72 o 2 6 0 67.07 -26.14 62.91 o 3 6 0 801.89 529.59 70.38 o 4 6 0 9759.15 9653.80 234.44 o 5 6 0 326.36 216.47 60.66 o 6 6 0 1176.16 1070.45 105.21 o 7 6 0 121.43 198.99 84.01 o 8 6 0 12817.39 12995.07 343.66 o 9 6 0 369.17 444.51 145.81 o 10 6 0 276.68 279.72 108.47 o 11 6 0 286.15 311.71 111.91 o 12 6 0 3293.36 3014.14 214.77 o 13 6 0 259.54 370.39 127.34 o 14 6 0 106.23 -151.45 231.52 o 0 7 0 96.22 241.71 114.56 o 1 7 0 16.57 62.45 88.34 o 2 7 0 158.79 92.86 81.26 o 3 7 0 735.51 737.07 105.25 o 4 7 0 2.37 217.48 114.13 o 5 7 0 1624.52 1587.53 163.58 o 6 7 0 3372.19 3160.98 223.98 o 7 7 0 287.76 225.54 118.34 o 8 7 0 33.06 248.91 149.57 o 9 7 0 172.20 310.18 139.37 o 10 7 0 1599.74 1567.88 190.55 o 11 7 0 221.43 214.98 141.54 o 12 7 0 27.13 477.87 228.67 o 0 8 0 11107.86 11614.73 519.94 o 1 8 0 374.55 207.31 98.35 o 2 8 0 1195.04 976.00 169.29 o 3 8 0 431.06 304.06 129.08 o 4 8 0 4525.99 4758.17 267.69 o 5 8 0 1140.02 1139.84 157.89 o 6 8 0 257.27 295.96 126.64 o 7 8 0 1093.86 981.97 194.65 o 8 8 0 2033.94 2580.54 344.08 o 9 8 0 1169.07 881.67 665.11 o 10 8 0 1320.47 2358.37 716.81 o 0 9 0 112.73 -135.72 210.80 o 1 9 0 12.03 -139.29 159.22 o 2 9 0 1126.21 1170.18 174.94 o 3 9 0 724.79 655.32 155.08 o 4 9 0 59.83 149.35 157.88 o 5 9 0 25.70 138.75 174.97 o -18 0 1 40.62 -240.02 240.02 o -16 0 1 562.11 665.12 195.80 o -14 0 1 282.03 289.35 122.98 o -12 0 1 7544.41 8244.13 238.21 o -10 0 1 3624.66 3705.59 102.91 o -8 0 1 4700.83 5245.01 106.32 o -6 0 1 281.96 192.15 43.37 o -4 0 1 3242.32 3281.18 72.29 o 2 0 1 1223.01 1010.10 39.35 o 4 0 1 48130.18 51819.91 461.42 o 6 0 1 8544.62 8857.31 161.64 o 8 0 1 612.03 758.87 53.82 o 10 0 1 62.46 17.70 51.82 o 12 0 1 817.32 762.22 94.08 o 14 0 1 1711.52 2139.12 257.83 o 16 0 1 2663.63 3076.95 337.98 o 18 0 1 336.49 958.45 533.25 o -19 1 1 1472.23 1220.06 341.42 o -18 1 1 6.28 -19.43 158.25 o -17 1 1 7.69 43.36 250.87 o -16 1 1 145.83 235.09 121.61 o -15 1 1 1592.02 1491.57 138.87 o -14 1 1 846.02 928.09 105.20 o -13 1 1 0.32 82.68 62.29 o -12 1 1 140.53 176.50 50.57 o -11 1 1 5332.88 4954.24 130.10 o -10 1 1 28.51 40.88 29.70 o -9 1 1 1973.90 1871.67 75.19 o -8 1 1 115.39 102.77 18.27 o -7 1 1 2.37 54.01 33.00 o -6 1 1 13610.89 14702.83 169.12 o -5 1 1 281.79 376.32 30.99 o -4 1 1 714.68 700.33 35.75 o -3 1 1 632.45 734.30 31.81 o -2 1 1 3112.25 3619.17 52.54 o -1 1 1 3177.24 3448.51 45.57 o 0 1 1 673.88 586.15 26.03 o 1 1 1 9333.28 9815.20 90.78 o 2 1 1 1956.46 2264.70 43.61 o 3 1 1 10540.93 10915.82 94.76 o 4 1 1 170.68 158.80 25.91 o 5 1 1 979.88 885.91 36.09 o 6 1 1 6563.76 6931.22 97.44 o 7 1 1 2550.97 2489.54 61.51 o 8 1 1 1214.70 1080.37 45.35 o 9 1 1 513.42 540.72 37.72 o 10 1 1 660.07 585.25 50.84 o 11 1 1 3263.02 3150.65 101.32 o 12 1 1 259.57 280.52 50.73 o 13 1 1 316.26 395.94 78.90 o 14 1 1 888.06 1010.75 108.58 o 15 1 1 43.10 79.76 145.12 o 16 1 1 111.53 206.45 140.01 o 17 1 1 38.02 -35.17 177.81 o -18 2 1 130.56 201.37 188.47 o -17 2 1 95.76 68.88 132.02 o -16 2 1 2148.22 2032.12 187.50 o -15 2 1 2.15 -97.85 106.73 o -14 2 1 2013.85 2213.89 143.94 o -13 2 1 83.72 76.80 80.00 o -12 2 1 107.24 27.04 68.53 o -11 2 1 1173.84 1156.14 89.56 o -10 2 1 442.98 389.70 59.86 o -9 2 1 259.66 248.19 51.37 o -8 2 1 686.17 668.31 39.57 o -7 2 1 1010.97 974.84 41.64 o -6 2 1 601.40 728.38 46.59 o -5 2 1 1074.42 1221.33 45.53 o -4 2 1 29503.12 30225.34 370.53 o -3 2 1 4.34 7.83 26.34 o -2 2 1 5580.62 5409.30 71.21 o -1 2 1 36.74 59.43 29.90 o 0 2 1 902.19 1279.68 45.55 o 1 2 1 1189.38 1174.59 37.89 o 2 2 1 38.34 99.53 26.03 o 3 2 1 2.21 32.54 26.87 o 4 2 1 50.11 123.27 28.36 o 5 2 1 3043.01 3440.29 74.40 o 6 2 1 1313.76 1209.92 49.65 o 7 2 1 323.21 260.48 30.65 o 8 2 1 4483.55 4488.52 104.70 o 9 2 1 84.37 119.62 38.82 o 10 2 1 27.18 27.02 42.56 o 11 2 1 130.77 143.09 50.47 o 12 2 1 4028.08 4171.80 175.08 o 13 2 1 8.95 173.19 90.37 o 14 2 1 298.69 557.74 135.58 o 15 2 1 22.28 293.54 124.90 o 16 2 1 221.82 167.69 150.18 o 17 2 1 3.59 -130.88 211.17 o -18 3 1 131.98 252.05 179.65 o -17 3 1 48.82 -103.87 133.17 o -16 3 1 68.11 -3.97 158.20 o -15 3 1 248.91 200.75 109.23 o -14 3 1 1826.26 1609.90 138.87 o -13 3 1 65.29 57.22 89.70 o -12 3 1 38.51 120.07 77.84 o -11 3 1 4963.71 4639.17 192.58 o -10 3 1 99.74 138.76 33.19 o -9 3 1 199.40 190.36 48.83 o -8 3 1 1456.98 1322.07 54.19 o -7 3 1 3322.86 3186.32 83.94 o -6 3 1 1108.05 1019.92 50.06 o -5 3 1 471.90 459.95 39.35 o -4 3 1 297.02 248.62 36.47 o -3 3 1 35.20 59.39 33.21 o -2 3 1 375.29 394.26 35.76 o -1 3 1 215.67 268.58 44.82 o 0 3 1 40.07 58.63 44.44 o 1 3 1 465.20 490.25 46.03 o 2 3 1 1262.60 1417.17 51.68 o 3 3 1 4337.49 4365.50 89.27 o 4 3 1 83.84 109.24 39.11 o 5 3 1 156.76 280.22 33.98 o 6 3 1 4794.43 4588.03 120.28 o 7 3 1 675.21 572.43 45.29 o 8 3 1 653.48 579.27 45.18 o 9 3 1 2480.06 2447.00 91.65 o 10 3 1 651.55 659.84 68.47 o 11 3 1 2901.15 2947.69 121.85 o 12 3 1 33.94 87.55 82.52 o 13 3 1 2.03 75.98 91.85 o 14 3 1 802.77 856.66 119.21 o 15 3 1 12.82 45.35 149.31 o 16 3 1 0.46 45.96 149.69 o 17 3 1 44.59 412.25 399.65 o -17 4 1 501.70 463.08 232.17 o -16 4 1 88.79 96.09 146.85 o -15 4 1 13.23 126.69 132.83 o -14 4 1 2.67 -36.20 101.27 o -13 4 1 8.56 -34.15 92.81 o -12 4 1 6736.61 6618.14 252.01 o -11 4 1 72.92 131.96 84.12 o -10 4 1 1530.02 1563.57 94.27 o -9 4 1 18.46 -11.96 47.60 o -8 4 1 2289.32 2391.51 94.41 o -7 4 1 2245.03 2273.15 101.88 o -6 4 1 3213.48 3131.89 113.64 o -5 4 1 446.97 520.64 57.78 o -4 4 1 254.75 322.23 47.84 o -3 4 1 2001.59 2125.49 83.66 o -2 4 1 60.76 81.85 36.82 o -1 4 1 4605.13 4758.48 145.09 o 0 4 1 581.63 690.41 59.97 o 1 4 1 1400.17 1361.43 77.20 o 2 4 1 778.96 729.60 57.28 o 3 4 1 205.94 198.19 44.97 o 4 4 1 16551.36 16995.22 242.30 o 5 4 1 248.44 256.56 44.15 o 6 4 1 251.30 250.33 42.98 o 7 4 1 0.58 -22.47 59.22 o 8 4 1 140.44 138.12 60.91 o 9 4 1 362.31 447.34 69.86 o 10 4 1 364.24 253.05 70.02 o 11 4 1 1287.96 1295.50 123.21 o 12 4 1 111.75 90.65 95.56 o 13 4 1 251.29 422.09 122.52 o 14 4 1 493.51 532.16 130.61 o 15 4 1 221.41 74.45 121.35 o 16 4 1 1153.50 987.75 216.43 o -16 5 1 187.75 -257.01 257.01 o -15 5 1 1151.44 1186.52 172.25 o -14 5 1 190.23 65.08 115.91 o -13 5 1 31.56 -40.95 111.32 o -12 5 1 137.01 37.27 110.08 o -11 5 1 1254.77 1271.52 137.63 o -10 5 1 1099.79 915.37 123.81 o -9 5 1 704.03 572.00 86.37 o -7 5 1 199.27 295.37 76.38 o -6 5 1 3571.24 3352.39 137.62 o -4 5 1 90.15 103.25 45.11 o -3 5 1 15.35 81.06 42.23 o -2 5 1 3795.84 3821.65 121.13 o -1 5 1 146.85 214.72 48.71 o 0 5 1 491.60 501.04 60.18 o 1 5 1 3742.05 3671.17 126.31 o 2 5 1 764.52 770.78 63.57 o 3 5 1 2245.14 2191.57 112.76 o 4 5 1 0.84 38.65 55.16 o 5 5 1 1314.85 1212.02 77.03 o 6 5 1 124.14 173.42 67.58 o 7 5 1 557.28 581.40 90.17 o 8 5 1 98.84 86.79 72.09 o 9 5 1 265.83 269.69 78.60 o 10 5 1 1.95 -109.50 109.50 o 11 5 1 1104.00 976.75 161.66 o 12 5 1 3.06 5.72 120.36 o 13 5 1 0.32 202.13 128.00 o 14 5 1 429.80 690.20 156.62 o 15 5 1 17.99 329.44 205.19 o -14 6 1 1567.67 1112.55 197.80 o -13 6 1 634.36 658.21 183.95 o -11 6 1 755.63 1184.33 148.09 o -10 6 1 31.79 60.56 100.00 o -9 6 1 1124.99 1054.55 124.77 o -8 6 1 28.94 131.80 88.17 o -7 6 1 425.86 551.06 84.85 o -6 6 1 867.86 846.90 90.81 o -5 6 1 37.40 58.09 60.52 o -4 6 1 10902.15 10887.26 276.06 o -3 6 1 4.33 112.62 63.30 o -2 6 1 417.97 448.84 79.46 o -1 6 1 585.03 597.69 78.31 o 0 6 1 659.76 495.64 58.95 o 1 6 1 1880.15 1988.11 101.73 o 2 6 1 153.08 197.09 67.53 o 3 6 1 1393.08 1410.66 100.57 o 4 6 1 61.65 119.96 61.99 o 5 6 1 702.95 791.46 99.16 o 6 6 1 317.42 271.77 91.61 o 7 6 1 974.92 922.78 110.53 o 8 6 1 1716.95 1687.86 131.02 o 9 6 1 565.45 572.75 120.22 o 10 6 1 395.70 368.31 145.52 o 11 6 1 45.11 9.86 115.03 o 12 6 1 1832.41 1627.97 168.30 o 13 6 1 67.92 26.91 174.16 o -13 7 1 149.76 1367.49 505.20 o -12 7 1 86.52 124.35 232.01 o -11 7 1 583.83 551.67 154.32 o -10 7 1 610.39 672.63 152.79 o -8 7 1 158.19 235.43 126.21 o -7 7 1 463.15 413.24 117.67 o -5 7 1 20.97 -25.67 105.75 o -4 7 1 307.54 278.84 114.31 o -3 7 1 32.77 100.99 90.20 o -2 7 1 11.42 -71.68 74.88 o -1 7 1 396.31 317.26 81.79 o 0 7 1 3.28 60.85 81.55 o 1 7 1 1314.33 1152.64 106.46 o 2 7 1 1135.84 1032.30 102.99 o 3 7 1 461.57 467.47 92.61 o 4 7 1 5.56 75.40 97.47 o 5 7 1 731.75 634.04 120.68 o 6 7 1 1189.04 1563.67 147.96 o 7 7 1 19.79 51.79 128.62 o 8 7 1 83.82 -5.80 176.90 o 9 7 1 269.41 285.93 151.57 o 10 7 1 182.86 265.04 203.85 o 11 7 1 863.98 1256.58 260.47 o -10 8 1 971.92 1297.69 658.72 o -9 8 1 508.11 495.84 359.58 o -8 8 1 551.57 529.31 154.51 o -7 8 1 875.72 685.37 165.75 o -6 8 1 1637.01 1424.55 177.22 o -5 8 1 1323.31 1222.32 163.41 o -4 8 1 65.13 96.98 128.89 o -3 8 1 380.30 190.20 126.32 o -2 8 1 562.72 621.49 113.73 o -1 8 1 1117.80 1115.05 129.41 o 0 8 1 289.90 305.20 106.58 o 1 8 1 295.88 401.53 112.88 o 2 8 1 1005.70 1004.92 162.75 o 3 8 1 173.53 -28.97 119.02 o 4 8 1 2731.95 2637.28 205.74 o 5 8 1 72.26 -17.11 127.90 o 6 8 1 234.14 69.39 135.43 o 7 8 1 434.75 548.93 167.39 o 8 8 1 195.26 124.15 252.49 o 9 8 1 846.30 40.66 575.07 o -6 9 1 1118.78 869.06 301.07 o -5 9 1 144.71 211.69 161.86 o -3 9 1 11.74 138.21 221.63 o -2 9 1 803.85 898.50 183.59 o -1 9 1 10.53 160.67 151.98 o 0 9 1 52.00 141.81 156.76 o 1 9 1 62.86 360.83 152.84 o 2 9 1 440.00 515.35 155.35 o 3 9 1 434.90 453.04 178.82 o 4 9 1 315.09 297.77 187.96 o 5 9 1 15.23 83.13 262.26 o -18 0 2 874.77 427.03 298.86 o -16 0 2 3816.71 3549.26 288.27 o -14 0 2 737.36 668.29 144.25 o -12 0 2 13328.62 13437.44 329.44 o -10 0 2 1.38 64.45 30.48 o -8 0 2 115627.32 123119.16 1056.15 o -6 0 2 109.60 225.43 32.40 o -4 0 2 41108.36 45311.81 462.40 o -2 0 2 1755.71 1312.54 43.41 o 0 0 2 28602.19 28594.32 343.67 o 2 0 2 1473.55 1216.63 56.08 o 4 0 2 14948.11 14486.69 207.69 o 6 0 2 2924.77 3278.86 122.04 o 8 0 2 18561.88 18955.40 331.50 o 10 0 2 167.35 191.28 66.58 o 12 0 2 4916.77 5107.69 224.74 o 14 0 2 1606.31 1591.50 225.78 o 16 0 2 6798.94 5928.12 530.44 o -19 1 2 666.00 501.10 321.68 o -18 1 2 581.78 990.39 187.75 o -17 1 2 16.77 132.13 129.39 o -16 1 2 224.71 561.73 177.42 o -15 1 2 397.57 515.27 95.04 o -14 1 2 2603.20 2640.03 152.36 o -13 1 2 15.06 71.17 57.19 o -12 1 2 63.27 46.55 50.89 o -11 1 2 4859.32 5405.70 150.01 o -10 1 2 4754.61 4664.62 113.70 o -9 1 2 521.72 435.40 38.18 o -8 1 2 365.48 280.49 35.26 o -7 1 2 859.57 1000.15 47.93 o -6 1 2 19144.06 19508.56 225.88 o -5 1 2 1804.38 1838.63 53.01 o -4 1 2 6.28 19.18 20.37 o -3 1 2 9905.05 11010.30 95.64 o -2 1 2 7530.50 6840.41 73.65 o -1 1 2 3528.33 3808.56 57.01 o 0 1 2 249.03 203.01 25.11 o 1 1 2 1977.75 1873.82 45.72 o 2 1 2 8055.14 7490.29 89.42 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503.51 33.98 o 0 2 2 128036.09 136836.08 1306.95 o 1 2 2 775.56 906.90 37.62 o 2 2 2 4.85 69.93 29.33 o 3 2 2 177.51 170.82 31.34 o 4 2 2 39968.95 41421.10 416.61 o 5 2 2 2661.66 2748.28 82.05 o 6 2 2 287.82 223.53 35.70 o 7 2 2 1.80 17.99 41.04 o 8 2 2 27510.74 27030.80 335.48 o 9 2 2 309.43 333.48 50.91 o 10 2 2 475.84 456.46 66.26 o 11 2 2 15.31 157.80 84.63 o 12 2 2 18333.79 18945.01 409.22 o 13 2 2 68.43 -1.00 146.64 o 14 2 2 29.41 -13.40 96.81 o 15 2 2 41.65 -25.60 117.96 o 16 2 2 3814.31 3779.84 292.66 o -18 3 2 662.72 576.55 230.61 o -17 3 2 263.65 131.91 136.03 o -16 3 2 197.23 44.59 120.30 o -15 3 2 792.19 705.51 103.49 o -14 3 2 3269.33 3499.52 194.93 o -13 3 2 17.54 118.19 89.16 o -12 3 2 152.97 92.71 65.73 o -11 3 2 4601.50 4622.03 168.98 o -10 3 2 798.62 857.30 88.89 o -9 3 2 11.96 37.00 28.81 o -8 3 2 37.86 81.41 32.45 o -7 3 2 78.53 89.21 29.87 o -6 3 2 3037.64 2531.02 71.82 o -5 3 2 120.83 102.03 29.66 o -4 3 2 56.02 56.32 29.15 o -3 3 2 4041.73 4015.65 86.38 o -2 3 2 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